Hexadecanoic acid (S)-2-{benzyloxy-[(1R,2R,3S,4R,5R,6S)-2,3,6-tris-benzyloxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-phosphoryloxy}-1-hexadecanoyloxymethyl-ethyl ester

Base Information

• Chemical Name: Hexadecanoic acid (S)-2-{benzyloxy-[(1R,2R,3S,4R,5R,6S)-2,3,6-tris-benzyloxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-phosphoryloxy}-1-hexadecanoyloxymethyl-ethyl ester
• CAS No.: 120595-87-1
• Molecular Formula: C₉₇H₁₂₉O₁₉P₃
• Molecular Weight: 1692

Synonyms:

Chemical Property of Hexadecanoic acid (S)-2-{benzyloxy-[(1R,2R,3S,4R,5R,6S)-2,3,6-tris-benzyloxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-phosphoryloxy}-1-hexadecanoyloxymethyl-ethyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Hexadecanoic acid (S)-2-{benzyloxy-[(1R,2R,3S,4R,5R,6S)-2,3,6-tris-benzyloxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-phosphoryloxy}-1-hexadecanoyloxymethyl-ethyl ester

There total 1 articles about Hexadecanoic acid (S)-2-{benzyloxy-[(1R,2R,3S,4R,5R,6S)-2,3,6-tris-benzyloxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-phosphoryloxy}-1-hexadecanoyloxymethyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Dibenzyl N,N-diisopropylphosphoramidite (108549-23-1) + Hexadecanoic acid (S)-2-[benzyloxy-((1S,2R,3R,4S,5S,6R)-2,3,6-tris-benzyloxy-4,5-dihydroxy-cyclohexyloxy)-phosphoryloxy]-1-hexadecanoyloxymethyl-ethyl ester (120615-72-7) → Hexadecanoic acid (S)-2-{benzyloxy-[(1R,2R,3S,4R,5R,6S)-2,3,6-tris-benzyloxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-phosphoryloxy}-1-hexadecanoyloxymethyl-ethyl ester (120595-87-1)

Guidance literature:

With 1H-tetrazole; tert.-butylhydroperoxide; Yield given. Multistep reaction;

DOI:10.1016/S0040-4039(00)82387-4

Reference yield:

Hexadecanoic acid (S)-2-{benzyloxy-[(1R,2R,3S,4R,5R,6S)-2,3,6-tris-benzyloxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-phosphoryloxy}-1-hexadecanoyloxymethyl-ethyl ester (120595-87-1) → Hexadecanoic acid (S)-1-hexadecanoyloxymethyl-2-[hydroxy-((1R,2R,3S,4R,6S)-2,3,6-trihydroxy-4,5-bis-phosphonooxy-cyclohexyloxy)-phosphoryloxy]-ethyl ester (120595-88-2,165883-85-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; chloroform; for 24h;

DOI:10.1016/S0040-4039(00)82387-4

upstream raw materials:

Dibenzyl N,N-diisopropylphosphoramidite

Hexadecanoic acid (S)-2-[benzyloxy-((1S,2R,3R,4S,5S,6R)-2,3,6-tris-benzyloxy-4,5-dihydroxy-cyclohexyloxy)-phosphoryloxy]-1-hexadecanoyloxymethyl-ethyl ester

Downstream raw materials:

Hexadecanoic acid (S)-1-hexadecanoyloxymethyl-2-[hydroxy-((1R,2R,3S,4R,6S)-2,3,6-trihydroxy-4,5-bis-phosphonooxy-cyclohexyloxy)-phosphoryloxy]-ethyl ester

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