[(C₁₂H₈N₂)((C₆H₅)3P)2Cu]⁽¹⁺⁾*[H₂B(O₂CH)2]^(1-)=[(C₁₂H₈N₂)((C₆H₅)3P)2Cu][H₂B(O₂CH)2]

Base Information

• Chemical Name: [(C₁₂H₈N₂)((C₆H₅)3P)2Cu]⁽¹⁺⁾*[H₂B(O₂CH)2]^(1-)=[(C₁₂H₈N₂)((C₆H₅)3P)2Cu][H₂B(O₂CH)2]
• CAS No.: 98482-03-2
• Molecular Formula: C₂H₄BO₄*C₄₈H₃₈CuN₂P₂
• Molecular Weight: 871.199

Synonyms:

Chemical Property of [(C₁₂H₈N₂)((C₆H₅)3P)2Cu]⁽¹⁺⁾*[H₂B(O₂CH)2]^(1-)=[(C₁₂H₈N₂)((C₆H₅)3P)2Cu][H₂B(O₂CH)2]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [(C₁₂H₈N₂)((C₆H₅)3P)2Cu]⁽¹⁺⁾*[H₂B(O₂CH)2]^(1-)=[(C₁₂H₈N₂)((C₆H₅)3P)2Cu][H₂B(O₂CH)2]

There total 2 articles about [(C₁₂H₈N₂)((C₆H₅)3P)2Cu]⁽¹⁺⁾*[H₂B(O₂CH)2]^(1-)=[(C₁₂H₈N₂)((C₆H₅)3P)2Cu][H₂B(O₂CH)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1,10-phenathroline)(triphenylphosphine)(tetrahydroborato)copper(I) (19581-73-8) → [(C12H8N2)((C6H5)3P)2Cu](1+)*[H2B(O2CH)2](1-)=[(C12H8N2)((C6H5)3P)2Cu][H2B(O2CH)2] (98482-03-2)

Guidance literature:

With CO₂; triphenyl phosphine; In dichloromethane; bubbling CO2 through a soln. of 3.1mmol PPh3 in 25ml CH2Cl2 at 40°C to which 0.52mmol Cu-complex was added, refluxing for 2h under CO2, removal of CH2Cl2 by bubbling CO2 through the soln.; mechanism discussed;; addn. of diethyl ether to the residue, refluxing for 30min., filtration, washing with diethyl ether, drying in vac.; elem. anal.;;

Reference yield:

[(C12H8N2)((C6H5)3P)2Cu](1+)*[HB(O2CH)3](1-)=[(C12H8N2)((C6H5)3P)2Cu][HB(O2CH)3] (98482-01-0) → [(C12H8N2)((C6H5)3P)2Cu](1+)*[H2B(O2CH)2](1-)=[(C12H8N2)((C6H5)3P)2Cu][H2B(O2CH)2] (98482-03-2)

Guidance literature:

In dichloromethane; byproducts: CO2; refluxing in degassed CH2Cl2 for 2.5h;; evapn.; treatment with ether, filtration; elem. anal.;;

Reference yield:

[(C12H8N2)((C6H5)3P)2Cu](1+)*[H2B(O2CH)2](1-)=[(C12H8N2)((C6H5)3P)2Cu][H2B(O2CH)2] (98482-03-2) → (1,10-phenanthroline)(triphenylphosphine)Cu(formate) (32474-61-6)

Guidance literature:

In ethanol; byproducts: H2, ethyl borate ester; heating at 45°C for 3h;;

upstream raw materials:

[(C₁₂H₈N₂)((C₆H₅)3P)2Cu]⁽¹⁺⁾*[HB(O₂CH)3]^(1-)=[(C₁₂H₈N₂)((C₆H₅)3P)2Cu][HB(O₂CH)3]

(1,10-phenathroline)(triphenylphosphine)(tetrahydroborato)copper(I)

Downstream raw materials:

(1,10-phenanthroline)(triphenylphosphine)Cu(formate)

[(C₁₂H₈N₂)((C₆H₅)3P)2Cu]⁽¹⁺⁾*[HB(O₂CH)3]^(1-)=[(C₁₂H₈N₂)((C₆H₅)3P)2Cu][HB(O₂CH)3]

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