C₃₂H₄₈N₂O₂*C₂₇H₃₁NO₅

Base Information

• Chemical Name: C₃₂H₄₈N₂O₂*C₂₇H₃₁NO₅
• CAS No.: 1599475-93-0
• Molecular Formula: C₂₇H₃₁NO₅*C₃₂H₄₈N₂O₂
• Molecular Weight: 942.292
• Mol file: 1599475-93-0.mol

Synonyms:

Chemical Property of C₃₂H₄₈N₂O₂*C₂₇H₃₁NO₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₃₂H₄₈N₂O₂*C₂₇H₃₁NO₅

There total 4 articles about C₃₂H₄₈N₂O₂*C₂₇H₃₁NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C27H31NO5 (1261359-52-7) + 2-amino-N-(3,5-di-tert-butylbenzyl)acetamide (1464148-90-0) + C28H44N2O2 (1464149-05-0) → C32H48N2O2*C27H31NO5 (1599475-93-0)

Guidance literature:

With sodium perchlorate; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1039/c3ob42418a

Reference yield:

1,4-bis(bromomethyl)benzene (623-24-5) → C32H48N2O2*C27H31NO5 (1599475-93-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C

1.2: 16 h / Reflux

2.1: sodium hydride; potassium carbonate / N,N-dimethyl-formamide / 168 h / 20 °C

3.1: sodium perchlorate / dichloromethane / 16 h / 20 °C

With sodium perchlorate; sodium hydride; potassium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1039/c3ob42418a

Reference yield:

ethylene glycol bis(4-bromomethylbenzyl) ether (1261359-51-6) → C32H48N2O2*C27H31NO5 (1599475-93-0)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride; potassium carbonate / N,N-dimethyl-formamide / 168 h / 20 °C

2: sodium perchlorate / dichloromethane / 16 h / 20 °C

With sodium perchlorate; sodium hydride; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1039/c3ob42418a

upstream raw materials:

1,4-bis(bromomethyl)benzene

C₂₇H₃₁NO₅

2-amino-N-(3,5-di-tert-butylbenzyl)acetamide

C₂₈H₄₄N₂O₂

Refernces