exo-Norbornylmethanol

Base Information

Chemical Name:exo-Norbornylmethanol
CAS No.:13118-79-1
Molecular Formula:C8H14O
Molecular Weight:126.199
Hs Code.:
UNII:VAV86MTU3Q
Nikkaji Number:J1.369.663B

Synonyms:exo-Norbornylmethanol;exo-2-Norbornanemethanol;VAV86MTU3Q;2-Norbornanemethanol, exo-;2-Hydroxymethylnorcamphane, exo-;UNII-VAV86MTU3Q;Bicyclo(2.2.1)heptane-2-methanol, exo-;exo-(+/-)-Bicyclo(2.2.1)heptane-2-methanol;13118-79-1;Bicyclo(2.2.1)heptane-2-methanol, (1R,2R,4S)-rel-

Suppliers and Price of exo-Norbornylmethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of exo-Norbornylmethanol

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:126.104465066
Heavy Atom Count:9
Complexity:111

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CC2CC1CC2CO
Isomeric SMILES:C1C[C@@H]2C[C@H]1C[C@H]2CO

Technology Process of exo-Norbornylmethanol

There total 9 articles about exo-Norbornylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 77-73-6,933-60-8,1755-01-7,25038-78-2
bi(cyclopentadiene)

: 934-30-5
exo-5-norbornene-2-carboxylic acid

: 13118-79-1
exo-2-Bicyclo<2.2.2>heptylmethanol

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 12h; Heating;
DOI:10.1002/chem.200501028

Reference yield: 60.0%

: 77-73-6,933-60-8,1755-01-7,25038-78-2
bi(cyclopentadiene)

: 1160212-03-2
H₂N-PEG₂₀₀₀-OMe

: 934-30-5
exo-5-norbornene-2-carboxylic acid

: 934-30-5
exo-5-norbornene-2-carboxylic acid

: 13118-79-1
exo-2-Bicyclo<2.2.2>heptylmethanol

: C₉₉H₁₉₂O₄₇

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 12h; Heating;
DOI:10.1002/chem.200501028

Reference yield:

: 120-74-1,934-30-5,1195-12-6,20507-53-3,58001-99-3,67999-50-2,67999-53-5,74645-32-2,108266-75-7
5-carboxybicyclo<2.2.1>hept-2-ene

: 13118-79-1
exo-2-Bicyclo<2.2.2>heptylmethanol

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / 1,2-dichloro-ethane / 2 h / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 40 °C

3: hydrogen; palladium 10% on activated carbon / ethyl acetate / 4.17 h / 20 °C

With dmap; lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1021/acs.jmedchem.0c00359