3-Amino-2-[6-(2-amino-3-phenyl-propionyloxy)-2,7-dimethoxy-1,4-dioxo-1,4-dihydro-carbazol-9-yl]-3-benzyl-1-(4-dimethylamino-phenyl)-4-oxo-azetidine-2-carboxylic acid methyl ester; hydrochloride

Base Information

Chemical Name:3-Amino-2-[6-(2-amino-3-phenyl-propionyloxy)-2,7-dimethoxy-1,4-dioxo-1,4-dihydro-carbazol-9-yl]-3-benzyl-1-(4-dimethylamino-phenyl)-4-oxo-azetidine-2-carboxylic acid methyl ester; hydrochloride
CAS No.:83317-59-3
Molecular Formula:C₄₃H₄₁N₅O₉*2ClH
Molecular Weight:844.749
Hs Code.:

3-Amino-2-[6-(2-amino-3-phenyl-propionyloxy)-2,7-dimethoxy-1,4-dioxo-1,4-dihydro-carbazol-9-yl]-3-benzyl-1-(4-dimethylamino-phenyl)-4-oxo-azetidine-2-carboxylic acid methyl ester; hydrochloride

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Chemical Property of 3-Amino-2-[6-(2-amino-3-phenyl-propionyloxy)-2,7-dimethoxy-1,4-dioxo-1,4-dihydro-carbazol-9-yl]-3-benzyl-1-(4-dimethylamino-phenyl)-4-oxo-azetidine-2-carboxylic acid methyl ester; hydrochloride

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Technology Process of 3-Amino-2-[6-(2-amino-3-phenyl-propionyloxy)-2,7-dimethoxy-1,4-dioxo-1,4-dihydro-carbazol-9-yl]-3-benzyl-1-(4-dimethylamino-phenyl)-4-oxo-azetidine-2-carboxylic acid methyl ester; hydrochloride

There total 5 articles about 3-Amino-2-[6-(2-amino-3-phenyl-propionyloxy)-2,7-dimethoxy-1,4-dioxo-1,4-dihydro-carbazol-9-yl]-3-benzyl-1-(4-dimethylamino-phenyl)-4-oxo-azetidine-2-carboxylic acid methyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 83317-53-7
3-Benzyl-1-(4-dimethylamino-phenyl)-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-{6-[2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-3-phenyl-propionyloxy]-2,7-dimethoxy-1,4-dioxo-1,4-dihydro-carbazol-9-yl}-4-oxo-azetidine-2-carboxylic acid methyl ester

: 83317-59-3
3-Amino-2-[6-(2-amino-3-phenyl-propionyloxy)-2,7-dimethoxy-1,4-dioxo-1,4-dihydro-carbazol-9-yl]-3-benzyl-1-(4-dimethylamino-phenyl)-4-oxo-azetidine-2-carboxylic acid methyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; hydrazine hydrate; In ethanol; for 2h; Heating;

Reference yield:

: 43042-33-7
4,4'-Dimethoxybiphenyl-2,5,2',5'-bis-p-benzoquinone

: 83317-59-3
3-Amino-2-[6-(2-amino-3-phenyl-propionyloxy)-2,7-dimethoxy-1,4-dioxo-1,4-dihydro-carbazol-9-yl]-3-benzyl-1-(4-dimethylamino-phenyl)-4-oxo-azetidine-2-carboxylic acid methyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / NaHCO₃ / ethanol; dioxane / 2 h / Heating

2: 100 percent / piperidine / ethanol / Heating

3: Et₃N / benzene

4: 38 percent / 1) N₂H₄*H₂O 2) HCl / ethanol / 2 h / Heating

With piperidine; hydrogenchloride; sodium hydrogencarbonate; hydrazine hydrate; triethylamine; In 1,4-dioxane; ethanol; benzene;

Reference yield:

: 83317-63-9
(6-Hydroxy-2,7-dimethoxy-1,4-dioxo-1,4-dihydro-carbazol-9-yl)-acetic acid methyl ester

: 83317-59-3
3-Amino-2-[6-(2-amino-3-phenyl-propionyloxy)-2,7-dimethoxy-1,4-dioxo-1,4-dihydro-carbazol-9-yl]-3-benzyl-1-(4-dimethylamino-phenyl)-4-oxo-azetidine-2-carboxylic acid methyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / piperidine / ethanol / Heating

2: Et₃N / benzene

3: 38 percent / 1) N₂H₄*H₂O 2) HCl / ethanol / 2 h / Heating

With piperidine; hydrogenchloride; hydrazine hydrate; triethylamine; In ethanol; benzene;