2, 2''',6,6'''-tetrachloro-1,1':2',1'':2'',1'''-quaterphenyl

Base Information

Chemical Name:2, 2''',6,6'''-tetrachloro-1,1':2',1'':2'',1'''-quaterphenyl
CAS No.:1612244-43-5
Molecular Formula:C₂₄H₁₄Cl₄
Molecular Weight:444.187
Hs Code.:

Synonyms:

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Chemical Property of 2, 2''',6,6'''-tetrachloro-1,1':2',1'':2'',1'''-quaterphenyl

Chemical Property:

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Technology Process of 2, 2''',6,6'''-tetrachloro-1,1':2',1'':2'',1'''-quaterphenyl

There total 3 articles about 2, 2''',6,6'''-tetrachloro-1,1':2',1'':2'',1'''-quaterphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33146-45-1
2,6-dichlorobiphenyl

: 1612244-43-5
2, 2''',6,6'''-tetrachloro-1,1':2',1'':2'',1'''-quaterphenyl

Guidance literature:: 2,6-dichlorobiphenyl; With copper(I) cyanide di(lithium chloride); In tetrahydrofuran; at -78 ℃; for 2h; Inert atmosphere; Sealed tube;

With oxygen; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; for 5h;
DOI:10.1021/ja504886x

Reference yield:

: 541-73-1
1,3-Dichlorobenzene

: 1612244-43-5
2, 2''',6,6'''-tetrachloro-1,1':2',1'':2'',1'''-quaterphenyl

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,2,6,6-tetramethylpiperidinyl-lithium / diethyl ether; tetrahydrofuran / 18 h / -78 °C / Sealed tube; Inert atmosphere

2.1: copper(I) cyanide di(lithium chloride) / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere; Sealed tube

2.2: 5 h / -78 - 20 °C

With copper(I) cyanide di(lithium chloride); 2,2,6,6-tetramethylpiperidinyl-lithium; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja504886x

Reference yield:

: 17763-67-6
Phenyl triflate

: 1612244-43-5
2, 2''',6,6'''-tetrachloro-1,1':2',1'':2'',1'''-quaterphenyl

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,2,6,6-tetramethylpiperidinyl-lithium / diethyl ether; tetrahydrofuran / 18 h / -78 °C / Sealed tube; Inert atmosphere

2.1: copper(I) cyanide di(lithium chloride) / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere; Sealed tube

2.2: 5 h / -78 - 20 °C

With copper(I) cyanide di(lithium chloride); 2,2,6,6-tetramethylpiperidinyl-lithium; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja504886x