thallium hydrotris(3-cyclohexylpyrazolil)borate

Base Information

Chemical Name:thallium hydrotris(3-cyclohexylpyrazolil)borate
CAS No.:163893-02-5
Molecular Formula:C₂₇H₄₀BN₆*Tl
Molecular Weight:663.849
Hs Code.:

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Chemical Property of thallium hydrotris(3-cyclohexylpyrazolil)borate

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Technology Process of thallium hydrotris(3-cyclohexylpyrazolil)borate

There total 1 articles about thallium hydrotris(3-cyclohexylpyrazolil)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: potassium borohydride

: thallium(I) nitrate

: 60061-66-7
3-cyclohexylpyrazole

: 163893-02-5
[(hydrotris(3-cyclohexylpyrazol-1-yl)borato)thallium(I)]

Guidance literature:: In neat (no solvent); byproducts: H2; heating of the pyrazole with KBH4, destn. (vac.), dissolving in DMF andreact. with TlNO3;

Reference yield: 85.0%

: nickel(II) chloride hexahydrate

: 163893-02-5
thallium hydrotris(3-cyclohexylpyrazolil)borate

: Ni(hydrotris(3-cyclohexylpyrazol-1-yl)borate)Cl

Guidance literature:: In water; acetonitrile; byproducts: TlCl; Tl-compound and NiCl2*6H2O ground to homogeneity in an agate mortar, then acetonitrile-water mixture added; mixture titurated for 5-6 min until an homogeneous blue mixture obtained; extrn. with toluene at 80°C, filtered free of TlCl and excess nickel chloride and diluted with hexane; cooled; crystals filtered off, washed with hexanes and dried in air; elem. anal.;
DOI:10.1016/j.inoche.2004.01.009

Reference yield: 82.0%

: 163893-02-5
[(hydrotris(3-cyclohexylpyrazol-1-yl)borato)thallium(I)]

: copper dichloride

: 163892-98-6
[(hydrotris(3-cyclohexylpyrazol-1-yl)borato)chloro-copper(II)]

Guidance literature:: In dichloromethane; stirring of the borato complex in CH2Cl2 with anhydrous CuCl2 for 20 min; filtn. through Celite and evapn. (vac.);