1,3,5-tri-(3,4,5-trihexylsulfanylphenyl)-6-oxoverdazyl

Base Information

Chemical Name:1,3,5-tri-(3,4,5-trihexylsulfanylphenyl)-6-oxoverdazyl
CAS No.:1355037-29-4
Molecular Formula:C₇₄H₁₂₃N₄OS₉
Molecular Weight:1373.41
Hs Code.:

Synonyms:

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Chemical Property of 1,3,5-tri-(3,4,5-trihexylsulfanylphenyl)-6-oxoverdazyl

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Technology Process of 1,3,5-tri-(3,4,5-trihexylsulfanylphenyl)-6-oxoverdazyl

There total 5 articles about 1,3,5-tri-(3,4,5-trihexylsulfanylphenyl)-6-oxoverdazyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1355037-37-4
2,4,6-tri(3,4,5-trihexylsulfanylphenyl)-1,2,4,5-tetrazane-3-one

: 1355037-29-4
1,3,5-tri-(3,4,5-trihexylsulfanylphenyl)-6-oxoverdazyl

Guidance literature:: With tetrabutylammomium bromide; sodium carbonate; potassium hexacyanoferrate(III); In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/ja209467h

Reference yield:

: 1355037-30-7
3,4,5-trihexylsulfanylphenylhydrazine

: 1355037-29-4
1,3,5-tri-(3,4,5-trihexylsulfanylphenyl)-6-oxoverdazyl

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / ethanol / 0.5 h / Reflux; Inert atmosphere

2: pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere

3: triethylamine / benzene / 2 h / 50 °C

4: tetrabutylammomium bromide; sodium carbonate; potassium hexacyanoferrate(III) / dichloromethane / 20 °C / Inert atmosphere

With pyridine; tetrabutylammomium bromide; sodium carbonate; acetic acid; triethylamine; potassium hexacyanoferrate(III); In ethanol; dichloromethane; benzene;
DOI:10.1021/ja209467h

Reference yield:

: 1355037-45-4
3,4,5-trihexylsulfanylbenzaldehyde 3,4,5-trihexylsulfanylphenylhydrazone

: 1355037-29-4
1,3,5-tri-(3,4,5-trihexylsulfanylphenyl)-6-oxoverdazyl

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere

2: triethylamine / benzene / 2 h / 50 °C

3: tetrabutylammomium bromide; sodium carbonate; potassium hexacyanoferrate(III) / dichloromethane / 20 °C / Inert atmosphere

With pyridine; tetrabutylammomium bromide; sodium carbonate; triethylamine; potassium hexacyanoferrate(III); In dichloromethane; benzene;
DOI:10.1021/ja209467h