[K(F₁₂-Tp^4Bo,3Ph)]

Base Information

Chemical Name:[K(F₁₂-Tp^4Bo,3Ph)]
CAS No.:1378981-72-6
Molecular Formula:C₃₉H₁₆BF₁₂N₆*K
Molecular Weight:846.486
Hs Code.:

[K(F<sub>12</sub>-Tp<sup>4Bo,3Ph</sup>)]

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Chemical Property of [K(F₁₂-Tp^4Bo,3Ph)]

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Technology Process of [K(F₁₂-Tp^4Bo,3Ph)]

There total 1 articles about [K(F₁₂-Tp^4Bo,3Ph)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: potassium borohydride

: 440096-20-8
3-phenyl-4,5,6,7-tetrafluoro-1H-indazole

: 1378981-72-6
[K(F₁₂-Tp^4Bo,3Ph)]

Guidance literature:: In neat (no solvent); (Schlenk, Ar) KBH4 was dried under vac. at 140°C for 1 h, KBH4 and indazole-compound were heated up to 190°C for 4 h, allowed to cool to room temp.; vac. sublimation, the residue was washed with methanol and dried under vac.;
DOI:10.1021/ic202125c

Reference yield: 68.0%

: thallium(I) sulfate

: 1378981-72-6
[K(F₁₂-Tp^4Bo,3Ph)]

: 1360075-80-4
[Tl(F₁₂-Tp^4Bo,3Ph)]

Guidance literature:: In chloroform; water; (Schlenk, Ar) a soln. of Tl2SO4 in water was added to a soln. of K-compound in CHCl3, the mixt. was stirred vigorously for 24 h; the organic layer was decanted, the water was extd. with CHCl3 (2x), evapd.; elem. anal.;
DOI:10.1021/ic202125c