7-hydroxy-trans-2-heptenoic acid

Base Information

Chemical Name:7-hydroxy-trans-2-heptenoic acid
CAS No.:66120-17-0
Molecular Formula:C₇H₁₂O₃
Molecular Weight:144.17
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-hydroxy-trans-2-heptenoic acid

Chemical Property:

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Technology Process of 7-hydroxy-trans-2-heptenoic acid

There total 1 articles about 7-hydroxy-trans-2-heptenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 694-54-2
tetrahydro-2H-2-pyranol

: 141-82-2
malonic acid

: 66120-17-0,10221-46-2
7-hydroxy-trans-2-heptenoic acid

: 13103-40-7
rac-2-(tetrahydro-2H-pyran-2-yl)acetic acid

Guidance literature:: piperidine; acetic acid; In dimethyl sulfoxide; 1.) r.t., 30 min, 2.) 100 deg C, 3 - 4 h;
DOI:10.1055/s-1993-25803

Reference yield:

: 66120-17-0,10221-46-2
7-hydroxy-trans-2-heptenoic acid

: 334-20-3,2575-01-1,29282-32-4
(E)-9-oxo-dec-2-enoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether

2: pyridine; phosphorus tribromide / benzene

3: sodium ethanolate / ethanol

4: sodium hydroxide / water

With pyridine; sodium ethanolate; phosphorus tribromide; sodium hydroxide; In diethyl ether; ethanol; water; benzene;
DOI:10.1007/s10600-011-0060-9

Reference yield:

: 66120-17-0,10221-46-2
7-hydroxy-trans-2-heptenoic acid

: 98206-48-5
[(1S,2S)-2-Cyano-2-(3-methoxy-phenyl)-cyclohexyl]-acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen chloride

2: pyridine / 1.) 0 deg C 2 min; 2.) to rt 6 h

3: potassium tert-butoxide / 2-methyl-propan-2-ol / 3 h / Heating

4: 20percent NaOH / methanol / 2.5 h / Heating

With hydrogenchloride; sodium hydroxide; potassium tert-butylate; In pyridine; methanol; tert-butyl alcohol;
DOI:10.1139/v85-172