C₂₁H₃₄O₅Si

Base Information

Chemical Name:C₂₁H₃₄O₅Si
CAS No.:1388153-26-1
Molecular Formula:C₂₁H₃₄O₅Si
Molecular Weight:394.583
Hs Code.:

C<sub>21</sub>H<sub>34</sub>O<sub>5</sub>Si

Synonyms:

Suppliers and Price of C₂₁H₃₄O₅Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of C₂₁H₃₄O₅Si

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of C₂₁H₃₄O₅Si

There total 11 articles about C₂₁H₃₄O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1388153-25-0
C₂₇H₄₈O₅Si₂

: 1388153-26-1
C₂₁H₃₄O₅Si

Guidance literature:: With camphor-10-sulfonic acid; In methanol; dichloromethane; at 0 ℃; for 5h;
DOI:10.1021/ja305864z

Reference yield:

: 1388152-88-2
C₁₄H₂₀O₄

: 1388153-26-1
C₂₁H₃₄O₅Si

Guidance literature:: Multi-step reaction with 9 steps

1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 20 °C

2: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.75 h / -78 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide / 0.67 h / 50 °C

4: diisobutylaluminium hydride / hexane; dichloromethane / 0.75 h / -78 °C / Inert atmosphere

5: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

6: tetrahydrofuran / 0.83 h / 20 °C

7: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C

8: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C

9: camphor-10-sulfonic acid / methanol; dichloromethane / 5 h / 0 °C

With 1H-imidazole; 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; camphor-10-sulfonic acid; dihydrogen peroxide; potassium hexamethylsilazane; diisobutylaluminium hydride; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja305864z

Reference yield:

: 1388152-90-6
C₁₆H₁₈O₅

: 1388153-26-1
C₂₁H₃₄O₅Si

Guidance literature:: Multi-step reaction with 6 steps

1: diisobutylaluminium hydride / hexane; dichloromethane / 0.75 h / -78 °C / Inert atmosphere

2: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

3: tetrahydrofuran / 0.83 h / 20 °C

4: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C

5: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C

6: camphor-10-sulfonic acid / methanol; dichloromethane / 5 h / 0 °C

With 1H-imidazole; 2,6-dimethylpyridine; camphor-10-sulfonic acid; dihydrogen peroxide; diisobutylaluminium hydride; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja305864z