(S)-2-{(S)-1-[(S)-1-Benzyl-2-(ethoxycarbonylmethyl-carbamoyl)-2-hydroxy-ethylcarbamoyl]-2-phenyl-ethylcarbamoyl}-5-oxo-pyrrolidine-1-carboxylic acid tert-butyl ester

Base Information

• Chemical Name: (S)-2-{(S)-1-[(S)-1-Benzyl-2-(ethoxycarbonylmethyl-carbamoyl)-2-hydroxy-ethylcarbamoyl]-2-phenyl-ethylcarbamoyl}-5-oxo-pyrrolidine-1-carboxylic acid tert-butyl ester
• CAS No.: 136138-86-8
• Molecular Formula: C₃₃H₄₂N₄O₉
• Molecular Weight: 638.718

Synonyms:

Chemical Property of (S)-2-{(S)-1-[(S)-1-Benzyl-2-(ethoxycarbonylmethyl-carbamoyl)-2-hydroxy-ethylcarbamoyl]-2-phenyl-ethylcarbamoyl}-5-oxo-pyrrolidine-1-carboxylic acid tert-butyl ester

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Technology Process of (S)-2-{(S)-1-[(S)-1-Benzyl-2-(ethoxycarbonylmethyl-carbamoyl)-2-hydroxy-ethylcarbamoyl]-2-phenyl-ethylcarbamoyl}-5-oxo-pyrrolidine-1-carboxylic acid tert-butyl ester

There total 1 articles about (S)-2-{(S)-1-[(S)-1-Benzyl-2-(ethoxycarbonylmethyl-carbamoyl)-2-hydroxy-ethylcarbamoyl]-2-phenyl-ethylcarbamoyl}-5-oxo-pyrrolidine-1-carboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Boc-pGlu-Phe-OH (99604-69-0) + ((S)-3-Amino-2-hydroxy-4-phenyl-butyrylamino)-acetic acid ethyl ester; hydrochloride (136138-84-6,136138-85-7) → (S)-2-{(S)-1-[(S)-1-Benzyl-2-(ethoxycarbonylmethyl-carbamoyl)-2-hydroxy-ethylcarbamoyl]-2-phenyl-ethylcarbamoyl}-5-oxo-pyrrolidine-1-carboxylic acid tert-butyl ester (136138-86-8,136233-28-8)

Guidance literature:

With 4-methyl-morpholine; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; Ambient temperature;

DOI:10.1016/0223-5234(91)90104-U

Reference yield:

(S)-2-{(S)-1-[(S)-1-Benzyl-2-(ethoxycarbonylmethyl-carbamoyl)-2-hydroxy-ethylcarbamoyl]-2-phenyl-ethylcarbamoyl}-5-oxo-pyrrolidine-1-carboxylic acid tert-butyl ester (136138-86-8,136233-28-8) → ((S)-2-Hydroxy-3-{(S)-2-[((S)-5-oxo-pyrrolidine-2-carbonyl)-amino]-3-phenyl-propionylamino}-4-phenyl-butyrylamino)-acetic acid ethyl ester (136138-89-1,136233-30-2)

Guidance literature:

With hydrogenchloride; In ethyl acetate; for 1h; Yield given; Ambient temperature;

DOI:10.1016/0223-5234(91)90104-U

upstream raw materials:

Boc-pGlu-Phe-OH

((S)-3-Amino-2-hydroxy-4-phenyl-butyrylamino)-acetic acid ethyl ester; hydrochloride

Downstream raw materials:

((S)-2-Hydroxy-3-{(S)-2-[((S)-5-oxo-pyrrolidine-2-carbonyl)-amino]-3-phenyl-propionylamino}-4-phenyl-butyrylamino)-acetic acid ethyl ester

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