Technology Process of trifluoroacetate of 1-(p-nitrophenyl)-2-butanol
There total 4 articles about trifluoroacetate of 1-(p-nitrophenyl)-2-butanol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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for 500h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 71 percent / triethylbenzylammonium chloride, KOH / 4 h / 40 °C
2: 76 percent / LiAlH4 / tetrahydrofuran / 10 h / Heating
3: 34.2 percent / HNO3(d=1.5) / acetic anhydride / 1 h / -50 °C
4: 28 percent / 500 h / Ambient temperature
With
potassium hydroxide; lithium aluminium tetrahydride; N-benzyl-N,N,N-triethylammonium chloride; nitric acid;
In
tetrahydrofuran; acetic anhydride;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 76 percent / LiAlH4 / tetrahydrofuran / 10 h / Heating
2: 34.2 percent / HNO3(d=1.5) / acetic anhydride / 1 h / -50 °C
3: 28 percent / 500 h / Ambient temperature
With
lithium aluminium tetrahydride; nitric acid;
In
tetrahydrofuran; acetic anhydride;
