Technology Process of 6,7,8,9,10,11-tribenzo-5,12-diphenyl-5,12-dihydro-5,12-epoxycyclooctanaphthalene
There total 3 articles about 6,7,8,9,10,11-tribenzo-5,12-diphenyl-5,12-dihydro-5,12-epoxycyclooctanaphthalene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 59 percent / Br2 / CCl4 / 1 h / Heating
2: 26 percent / KOtBu / diethyl ether / 72 h
With
potassium tert-butylate; bromine;
In
tetrachloromethane; diethyl ether;
DOI:10.1016/S0040-4020(01)88542-2
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 31 percent / NBS, dibenzoyl peroxide / CCl4 / 2.5 h / Heating
2: 48 percent / KOt-Bu / tetrahydrofuran / 0 h
With
N-Bromosuccinimide; potassium tert-butylate; dibenzoyl peroxide;
In
tetrahydrofuran; tetrachloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 60 percent / 1.5 h / 150 - 160 °C
2: 31 percent / NBS, dibenzoyl peroxide / CCl4 / 2.5 h / Heating
3: 48 percent / KOt-Bu / tetrahydrofuran / 0 h
With
N-Bromosuccinimide; potassium tert-butylate; dibenzoyl peroxide;
In
tetrahydrofuran; tetrachloromethane;
