(S)-3-Amino-N-{(S)-1-[(S)-2-tert-butoxy-1-((S)-1-phenoxycarbonyl-ethylcarbamoyl)-ethylcarbamoyl]-2-methyl-propyl}-succinamic acid tert-butyl ester; compound with toluene-4-sulfonic acid

Base Information

Chemical Name:(S)-3-Amino-N-{(S)-1-[(S)-2-tert-butoxy-1-((S)-1-phenoxycarbonyl-ethylcarbamoyl)-ethylcarbamoyl]-2-methyl-propyl}-succinamic acid tert-butyl ester; compound with toluene-4-sulfonic acid
CAS No.:80682-43-5
Molecular Formula:C₇H₈O₃S*C₂₉H₄₆N₄O₈
Molecular Weight:750.911
Hs Code.:

(S)-3-Amino-N-{(S)-1-[(S)-2-tert-butoxy-1-((S)-1-phenoxycarbonyl-ethylcarbamoyl)-ethylcarbamoyl]-2-methyl-propyl}-succinamic acid tert-butyl ester; compound with toluene-4-sulfonic acid

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Chemical Property of (S)-3-Amino-N-{(S)-1-[(S)-2-tert-butoxy-1-((S)-1-phenoxycarbonyl-ethylcarbamoyl)-ethylcarbamoyl]-2-methyl-propyl}-succinamic acid tert-butyl ester; compound with toluene-4-sulfonic acid

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Technology Process of (S)-3-Amino-N-{(S)-1-[(S)-2-tert-butoxy-1-((S)-1-phenoxycarbonyl-ethylcarbamoyl)-ethylcarbamoyl]-2-methyl-propyl}-succinamic acid tert-butyl ester; compound with toluene-4-sulfonic acid

There total 1 articles about (S)-3-Amino-N-{(S)-1-[(S)-2-tert-butoxy-1-((S)-1-phenoxycarbonyl-ethylcarbamoyl)-ethylcarbamoyl]-2-methyl-propyl}-succinamic acid tert-butyl ester; compound with toluene-4-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-15-4
toluene-4-sulfonic acid

: 80682-25-3
Z-Asp(OtBu)-Val-Ser(tBu)-Ala-OPh

: 80682-43-5
(S)-3-Amino-N-{(S)-1-[(S)-2-tert-butoxy-1-((S)-1-phenoxycarbonyl-ethylcarbamoyl)-ethylcarbamoyl]-2-methyl-propyl}-succinamic acid tert-butyl ester; compound with toluene-4-sulfonic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide; for 5h;
DOI:10.1016/S0040-4020(01)98919-7

Reference yield:

: 80682-43-5
(S)-3-Amino-N-{(S)-1-[(S)-2-tert-butoxy-1-((S)-1-phenoxycarbonyl-ethylcarbamoyl)-ethylcarbamoyl]-2-methyl-propyl}-succinamic acid tert-butyl ester; compound with toluene-4-sulfonic acid

: 47634-33-3
Bpoc-Ser(Bu^t)-OH

: 80682-26-4
Bpoc-Ser(tBu)-Asp(OtBu)-Val-Ser(tBu)-Ala-OPh

Guidance literature:: With 4-methyl-morpholine; 1-hydroxy-pyrrolidine-2,5-dione; μ-Oxo-bis-; Yield given. Multistep reaction; 1.) DMF, -5 deg C, 2.) DMF, room temperature;
DOI:10.1016/S0040-4020(01)98919-7