C₆₄H₄₂O₂

Base Information

Chemical Name:C₆₄H₄₂O₂
CAS No.:1613039-61-4
Molecular Formula:C₆₄H₄₂O₂
Molecular Weight:843.036
Hs Code.:

C<sub>64</sub>H<sub>42</sub>O<sub>2</sub>

Synonyms:

Suppliers and Price of C₆₄H₄₂O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₄H₄₂O₂

Chemical Property:

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Technology Process of C₆₄H₄₂O₂

There total 8 articles about C₆₄H₄₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1612866-62-2
2-(3,5-diphenylphenyl)phenanthren-4-ol

: 1613039-61-4,1613039-62-5,1613040-51-9
C₆₄H₄₂O₂

Guidance literature:: With air; In mineral oil; at 195 ℃; for 12h;
DOI:10.1002/anie.201310491

Reference yield:

: 19752-57-9
1,3-dibromo-5-iodobenzene

: 1613039-61-4,1613039-62-5,1613040-51-9
C₆₄H₄₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: bis-triphenylphosphine-palladium(II) chloride; triethylamine; copper(l) chloride / tetrahydrofuran / 0.08 h / 20 °C / Inert atmosphere

1.2: 27 h / 20 °C / Inert atmosphere

2.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 48 h / 65 °C / Inert atmosphere

3.1: potassium carbonate / methanol / 25 h / 20 °C

4.1: 2-Methylpropionic anhydride / 48 h / 190 °C / Inert atmosphere

4.2: 60 - 100 °C

5.1: air / mineral oil / 12 h / 195 °C

With bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2-Methylpropionic anhydride; potassium carbonate; triethylamine; copper(l) chloride; In tetrahydrofuran; methanol; mineral oil;
DOI:10.1002/anie.201310491

Reference yield:

: 135853-29-1
3',5'-dibromo-2-phenyl-1-(trimethylsilyl)acetylene

: 1613039-61-4,1613039-62-5,1613040-51-9
C₆₄H₄₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 48 h / 65 °C / Inert atmosphere

2.1: potassium carbonate / methanol / 25 h / 20 °C

3.1: 2-Methylpropionic anhydride / 48 h / 190 °C / Inert atmosphere

3.2: 60 - 100 °C

4.1: air / mineral oil / 12 h / 195 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2-Methylpropionic anhydride; potassium carbonate; In tetrahydrofuran; methanol; mineral oil;
DOI:10.1002/anie.201310491