C₂₉H₃₅NO₇Si

Base Information

Chemical Name:C₂₉H₃₅NO₇Si
CAS No.:1400814-11-0
Molecular Formula:C₂₉H₃₅NO₇Si
Molecular Weight:537.685
Hs Code.:

C<sub>29</sub>H<sub>35</sub>NO<sub>7</sub>Si

Synonyms:

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Chemical Property of C₂₉H₃₅NO₇Si

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Technology Process of C₂₉H₃₅NO₇Si

There total 5 articles about C₂₉H₃₅NO₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: C₂₇H₃₃NO₆Si

: 108-24-7
acetic anhydride

: 1400814-11-0
C₂₉H₃₅NO₇Si

Guidance literature:: With dmap; triethylamine; In dichloromethane;
DOI:10.1271/bbb.120134

Reference yield:

: 1301166-50-6
(4R)-4-[(1S)-1-methoxymethoxy-3-buten-1-yl]-2,2-dimethyl-1,3-dioxolane

: 1400814-11-0
C₂₉H₃₅NO₇Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: water; pyridinium p-toluenesulfonate / methanol / 5 h / 20 - 60 °C

2.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

3.2: 16 h / -78 - 0 °C / Inert atmosphere

4.1: potassium carbonate / tetrahydrofuran; methanol / 2.33 h / 20 °C / Reflux

5.1: zinc dibromide; 1-dodecylthiol / dichloromethane / 0.5 h / 20 °C

6.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h / 20 °C

7.1: dimethylsulfide; sodium hydrogencarbonate; ozone / methanol; dichloromethane

8.1: dmap; triethylamine / dichloromethane

With 1H-imidazole; dmap; dimethylsulfide; water; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; ozone; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; zinc dibromide; 1-dodecylthiol; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; 3.1: Dess-Martin oxidation;
DOI:10.1271/bbb.120134

Reference yield:

: 1332623-02-5
(2R,3S)-1-(tert-butyldiphenylsilyloxy)-3-methoxymethoxy-5-hexen-2-ol

: 1400814-11-0
C₂₉H₃₅NO₇Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

1.2: 16 h / -78 - 0 °C / Inert atmosphere

2.1: potassium carbonate / tetrahydrofuran; methanol / 2.33 h / 20 °C / Reflux

3.1: zinc dibromide; 1-dodecylthiol / dichloromethane / 0.5 h / 20 °C

4.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h / 20 °C

5.1: dimethylsulfide; sodium hydrogencarbonate; ozone / methanol; dichloromethane

6.1: dmap; triethylamine / dichloromethane

With dmap; dimethylsulfide; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; ozone; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; zinc dibromide; 1-dodecylthiol; In tetrahydrofuran; methanol; dichloromethane; 1.1: Dess-Martin oxidation;
DOI:10.1271/bbb.120134