N-p-methoxybenzyloxycarbonyl-L-leucine azide

Base Information

Chemical Name:N-p-methoxybenzyloxycarbonyl-L-leucine azide
CAS No.:102195-78-8
Molecular Formula:C₁₅H₂₀N₄O₄
Molecular Weight:320.348
Hs Code.:

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Chemical Property of N-p-methoxybenzyloxycarbonyl-L-leucine azide

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Technology Process of N-p-methoxybenzyloxycarbonyl-L-leucine azide

There total 3 articles about N-p-methoxybenzyloxycarbonyl-L-leucine azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88491-32-1
N-p-methoxybenzyloxycarbonyl-L-leucine hydrazide

: 102195-78-8
N-p-methoxybenzyloxycarbonyl-L-leucine azide

Guidance literature:: With hydrogenchloride; tert.-butylnitrite; In tetrahydrofuran; diethyl ether; at -15 ℃; for 0.5h;

Reference yield:

: 21209-49-4
N-p-methoxybenzyloxycarbonyl-L-leucine dicyclohexylammonium salt

: 102195-78-8
N-p-methoxybenzyloxycarbonyl-L-leucine azide

Guidance literature:: Multi-step reaction with 3 steps

1: H₂SO₄ / diethyl ether; H₂O

2: hydrazine hydrate / methanol / 3 h / r.t.-> 4 deg C

3: HCl, t-butyl nitrite / tetrahydrofuran; diethyl ether / 0.5 h / -15 °C

With hydrogenchloride; tert.-butylnitrite; sulfuric acid; hydrazine hydrate; In tetrahydrofuran; methanol; diethyl ether; water;

Reference yield:

: 62188-78-7
N-p-methoxybenzyloxycarbonyl-L-leucine methyl ester

: 102195-78-8
N-p-methoxybenzyloxycarbonyl-L-leucine azide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / 3 h / r.t.-> 4 deg C

2: HCl, t-butyl nitrite / tetrahydrofuran; diethyl ether / 0.5 h / -15 °C

With hydrogenchloride; tert.-butylnitrite; hydrazine hydrate; In tetrahydrofuran; methanol; diethyl ether;