(C₅(C₆H₅)5)Ru(C₁₀H₁₁N₂)

Base Information

• Chemical Name: (C₅(C₆H₅)5)Ru(C₁₀H₁₁N₂)
• CAS No.: 211989-01-4
• Molecular Formula: C₄₅H₃₆N₂Ru
• Molecular Weight: 705.864

Synonyms:

Chemical Property of (C₅(C₆H₅)5)Ru(C₁₀H₁₁N₂)

Chemical Property:

Purity/Quality:

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Technology Process of (C₅(C₆H₅)5)Ru(C₁₀H₁₁N₂)

There total 1 articles about (C₅(C₆H₅)5)Ru(C₁₀H₁₁N₂) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

N,N-dimethyl-7H-cyclopenta[b]pyridine-4-amine (183619-58-1) + bromodicarbonyl(η-pentaphenylcyclopentadienyl)ruthenium → (C5(C6H5)5)Ru(C10H11N2) (211989-01-4,212080-20-1)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; hexane; (inert atmosphere); addn. of n-BuLi (in hexane) to the pyrindine in toluene, stirring (room temp., 1 h), addn. of the Ru complex in toluene, reflux, 22 h, cooling to room temp.; concn. of reaction mixture, extraction of residue (Et2O/H2O), passing org. layer through alumina, concn., flash chomy. (SiO2, 50% EtOAc/hexane-> 10% NEt3/EtOAc), enantiomeric mixture; elem. anal.;

DOI:10.1021/ja981061o

upstream raw materials:

N,N-dimethyl-7H-cyclopenta[b]pyridine-4-amine

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