Fc(SiMe₂)2(C₆H₄-p-OMe)

Base Information

• Chemical Name: Fc(SiMe₂)2(C₆H₄-p-OMe)
• CAS No.: 260995-63-9
• Molecular Formula: C₂₁H₂₈FeOSi₂
• Molecular Weight: 408.471

Synonyms:

Chemical Property of Fc(SiMe₂)2(C₆H₄-p-OMe)

Chemical Property:

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Technology Process of Fc(SiMe₂)2(C₆H₄-p-OMe)

There total 1 articles about Fc(SiMe₂)2(C₆H₄-p-OMe) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(chloromercuri)ferrocene + 1-chloro-2-(4-methoxyphenyl)-1,1,2,2-tetramethyldisilane (133947-05-4) → Fc(SiMe2)2(C6H4-p-OMe) (260995-63-9)

Guidance literature:

With n-BuLi; In tetrahydrofuran; byproducts: LiCl, (n-Bu)2Hg; all manipulations under Ar; soln. of ferrocenyllithium ( prepared from n-BuLi and chloromercurioferrocene) in THF) added to soln. of Si compd. in THF at -25°C, stirred for 30 min,, warmed to room temp., stirred for 12 h, solvent removed in vac.; residue extd. with hexane, filtered, filtrate concd., Hg compd. removed by distn. in vac., residue purified by molecular distn., elem. anal.;

DOI:10.1021/om990733w

upstream raw materials:

1-chloro-2-(4-methoxyphenyl)-1,1,2,2-tetramethyldisilane

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