α-chloro-α-butylcaproic acid phenylhydrazide

Base Information

• Chemical Name: α-chloro-α-butylcaproic acid phenylhydrazide
• CAS No.: 95101-58-9
• Molecular Formula: C₁₆H₂₅ClN₂O
• Molecular Weight: 296.84
• Mol file: 95101-58-9.mol

Synonyms:

Chemical Property of α-chloro-α-butylcaproic acid phenylhydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α-chloro-α-butylcaproic acid phenylhydrazide

There total 1 articles about α-chloro-α-butylcaproic acid phenylhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dibutylglycolic acid phenylhydrazide (3178-55-0) → α-chloro-α-butylcaproic acid phenylhydrazide (95101-58-9)

Guidance literature:

With phosphorus pentachloride; In 1,4-dioxane; at 20 ℃; Yield given;

Reference yield: 64.0%

α-chloro-α-butylcaproic acid phenylhydrazide (95101-58-9) → 2-butyl-hex-2-enoic acid N'-phenyl-hydrazide

Guidance literature:

With phenol; at 120 - 130 ℃; for 0.05h;

DOI:10.1023/A:1010497526993

Reference yield: 50.0%

n-butanethiol (109-79-5) + α-chloro-α-butylcaproic acid phenylhydrazide (95101-58-9) → α-butylthio-α-butylcaproic acid phenylhydrazide

Guidance literature:

With phenol; In methanol; for 3h;

DOI:10.1023/A:1010497526993

upstream raw materials:

dibutylglycolic acid phenylhydrazide

Refernces