[N-methylpyridinium][Au(triphenylphosphine)(2-((4,5-ethylenedithio)-1,3-dithiole-2-ylidene)-1,3-dithiole-4,5-dithionato)]

Base Information

• Chemical Name: [N-methylpyridinium][Au(triphenylphosphine)(2-((4,5-ethylenedithio)-1,3-dithiole-2-ylidene)-1,3-dithiole-4,5-dithionato)]
• CAS No.: 782500-50-9
• Molecular Formula: C₆H₈N*C₂₆H₁₉AuPS₈
• Molecular Weight: 910.041
• Mol file: 782500-50-9.mol

Synonyms:

Chemical Property of [N-methylpyridinium][Au(triphenylphosphine)(2-((4,5-ethylenedithio)-1,3-dithiole-2-ylidene)-1,3-dithiole-4,5-dithionato)]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [N-methylpyridinium][Au(triphenylphosphine)(2-((4,5-ethylenedithio)-1,3-dithiole-2-ylidene)-1,3-dithiole-4,5-dithionato)]

There total 1 articles about [N-methylpyridinium][Au(triphenylphosphine)(2-((4,5-ethylenedithio)-1,3-dithiole-2-ylidene)-1,3-dithiole-4,5-dithionato)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

(triphenylphosphine)gold(I) chloride (14243-64-2) + N-methylpyridinium chloride (7680-73-1) + 4,5-bis(cyanoethylthio)-1,3-dithiole-2-[(4,5-ethylenedithio)-1,3-dithiole-2-ylidene] (158871-27-3) → [N-methylpyridinium][Au(triphenylphosphine)(2-((4,5-ethylenedithio)-1,3-dithiole-2-ylidene)-1,3-dithiole-4,5-dithionato)] (782500-50-9)

Guidance literature:

With Na; In ethanol; dichloromethane; (Ar); dissolving of C8H4S8(CH2CH2CN)2 in EtOH soln. containing Na; addn.with stirring of soln. of AuCl(PEt3) and N-methylpyridinium chloride in CH2Cl2; stirring for 30 min; pptn., filtration, washing with CH2Cl2 and MeOH, drying in vac., elem. anal.;

DOI:10.1016/j.ica.2004.03.048

upstream raw materials:

(triphenylphosphine)gold(I) chloride

N-methylpyridinium chloride

4,5-bis(cyanoethylthio)-1,3-dithiole-2-[(4,5-ethylenedithio)-1,3-dithiole-2-ylidene]