Gd(C₆H₅N₂C₃(CH₃)2(CHO)O)4I₂⁽¹⁺⁾*I^(1-)=[Gd(C₆H₅N₂C₃(CH₃)2(CHO)O)4I₂]I

Base Information

Chemical Name:Gd(C₆H₅N₂C₃(CH₃)2(CHO)O)4I₂⁽¹⁺⁾*I^(1-)=[Gd(C₆H₅N₂C₃(CH₃)2(CHO)O)4I₂]I
CAS No.:242489-96-9
Molecular Formula:C₄₈H₄₈GdI₂N₈O₈*I
Molecular Weight:1402.92
Hs Code.:

Gd(C<sub>6</sub>H<sub>5</sub>N<sub>2</sub>C<sub>3</sub>(CH<sub>3</sub>)2(CHO)O)4I<sub>2</sub><sup>(1+)</sup>*I<sup>(1-)</sup>=[Gd(C<sub>6</sub>H<sub>5</sub>N<sub>2</sub>C<sub>3</sub>(CH<sub>3</sub>)2(CHO)O)4I<sub>2</sub>]I

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Chemical Property of Gd(C₆H₅N₂C₃(CH₃)2(CHO)O)4I₂⁽¹⁺⁾*I^(1-)=[Gd(C₆H₅N₂C₃(CH₃)2(CHO)O)4I₂]I

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Technology Process of Gd(C₆H₅N₂C₃(CH₃)2(CHO)O)4I₂⁽¹⁺⁾*I^(1-)=[Gd(C₆H₅N₂C₃(CH₃)2(CHO)O)4I₂]I

There total 1 articles about Gd(C₆H₅N₂C₃(CH₃)2(CHO)O)4I₂⁽¹⁺⁾*I^(1-)=[Gd(C₆H₅N₂C₃(CH₃)2(CHO)O)4I₂]I which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 13572-98-0
gadolinium(III) iodide

: 950-81-2
4-formyl-2,3-dimethyl-1-phenyl-3-pyrazolin-5-one

: 242489-96-9
Gd(C₆H₅N₂C₃(CH₃)2(CHO)O)4I₂⁽¹⁺⁾*I^(1-)=[Gd(C₆H₅N₂C₃(CH₃)2(CHO)O)4I₂]I

Guidance literature:: In methanol; acetonitrile; addn. of soln. of LnI3 in MeOH to soln. of org. ligand in MeCN (small excess of org. ligand), refluxing (8 h), filtration, evapn. to viscous mass; washing (hot CHCl3), dissoln. of solid complex in MeCN, addn. of a few drops of benzene to satd. soln. (stirring; crystn.), filtration, drying (over P2O5, vac.); elem. anal.;
DOI:10.1080/00945719909349523