-(RS)-isoleucinylnitrile

Base Information

Chemical Name:-(RS)-isoleucinylnitrile
CAS No.:132402-75-6
Molecular Formula:C₁₈H₂₅N₃O₄
Molecular Weight:347.414
Hs Code.:

<N-benzyloxycarbonyl-(S)-threonyl>-(RS)-isoleucinylnitrile

Synonyms:

Suppliers and Price of -(RS)-isoleucinylnitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of -(RS)-isoleucinylnitrile

Chemical Property:

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Technology Process of -(RS)-isoleucinylnitrile

There total 2 articles about -(RS)-isoleucinylnitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 128203-33-8
(RS)-isoleucinylnitrile

: 19728-63-3
N-benzyloxycarbonyl-L-treonine

: 132402-75-6,132487-33-3
-(RS)-isoleucinylnitrile

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; for 18h; Ambient temperature;
DOI:10.1016/S0040-4020(01)81482-4

Reference yield:

: 96-17-3,57456-98-1
2-Methylbutyraldehyde

: 132402-75-6,132487-33-3
-(RS)-isoleucinylnitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / NH₄OAc / ethanol / 18 h / Ambient temperature

2: 94 percent / N-hydroxybenzotriazole, dicyclohexylcarbodiimide / CH₂Cl₂ / 18 h / Ambient temperature

With ammonium acetate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)81482-4

Reference yield:

: 132402-75-6,132487-33-3
-(RS)-isoleucinylnitrile

: 132402-77-8,132487-35-5
(R)-2-[1-((2S,3R)-2-Benzyloxycarbonylamino-3-hydroxy-butyrylamino)-2-methyl-butyl]-4,5-dihydro-thiazole-4-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / diethyl ether / Ambient temperature

2: 21 percent / ethanol / Ambient temperature

With hydrogenchloride; In diethyl ether; ethanol;
DOI:10.1016/S0040-4020(01)81482-4