C₂₆H₃₁NO₂

Base Information

Chemical Name:C₂₆H₃₁NO₂
CAS No.:128097-44-9
Molecular Formula:C₂₆H₃₁NO₂
Molecular Weight:389.538
Hs Code.:

C<sub>26</sub>H<sub>31</sub>NO<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₃₁NO₂

Chemical Property:

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Technology Process of C₂₆H₃₁NO₂

There total 11 articles about C₂₆H₃₁NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 128097-44-9,128163-72-4
C₂₆H₃₁NO₂

: 128097-44-9,128163-72-4
C₂₆H₃₁NO₂

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; at -15 ℃; for 1h;
DOI:10.1007/BF00506857

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 128097-44-9,128163-72-4
C₂₆H₃₁NO₂

Guidance literature:: Multi-step reaction with 3 steps

1: 1) dimethylamine hydrochloride, conc.HCl / 1) i-PrOH, reflux, 1 h, 2) reflux, 15 h

2: 89 percent / hexachloroethane / xylene / 1 h / Heating

3: 2) 30percent H₂O₂, AcONa/AcOH / 1) THF, reflux, 30 min, 2) THF, PrOH, -10 deg C, 15 h

With hydrogenchloride; hexachloroethane; dihydrogen peroxide; N,N-dimethylammonium chloride; sodium acetate; acetic acid; In xylene;
DOI:10.1007/BF00506857

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 128097-44-9,128163-72-4
C₂₆H₃₁NO₂

Guidance literature:: Multi-step reaction with 4 steps

1: 1) dimethylamine hydrochloride, conc.HCl / 1) i-PrOH, reflux, 1 h, 2) reflux, 15 h

2: 89 percent / hexachloroethane / xylene / 1 h / Heating

3: 2) 30percent H₂O₂, AcONa/AcOH / 1) THF, reflux, 30 min, 2) THF, PrOH, -10 deg C, 15 h

4: 100 percent / conc.HCl / tetrahydrofuran / 1 h / -15 °C

With hydrogenchloride; hexachloroethane; dihydrogen peroxide; N,N-dimethylammonium chloride; sodium acetate; acetic acid; In tetrahydrofuran; xylene;
DOI:10.1007/BF00506857