2,6-[(2,6-iPr₂C₆H₃)NC(CH(CH₃)2)]2C₅H₃N iron dichloride

Base Information

• Chemical Name: 2,6-[(2,6-iPr₂C₆H₃)NC(CH(CH₃)2)]2C₅H₃N iron dichloride
• CAS No.: 332390-58-6
• Molecular Formula: C₃₇H₅₁Cl₂FeN₃
• Molecular Weight: 664.585
• Mol file: 332390-58-6.mol

Synonyms:

Chemical Property of 2,6-[(2,6-iPr₂C₆H₃)NC(CH(CH₃)2)]2C₅H₃N iron dichloride

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2,6-[(2,6-iPr₂C₆H₃)NC(CH(CH₃)2)]2C₅H₃N iron dichloride

There total 1 articles about 2,6-[(2,6-iPr₂C₆H₃)NC(CH(CH₃)2)]2C₅H₃N iron dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

2,6-[(2,6-iPr2C6H3)NC(CH(CH3)2)]2C5H3N (332391-00-1) + water (7732-18-5) + iron(II) chloride → 2,6-[(2,6-iPr2C6H3)NC(CH(CH3)2)]2C5H3N iron dichloride (332390-58-6)

Guidance literature:

In butan-1-ol; (N2), stoich., suspn. of ligand in n-butanol added dropwise at 80°C to FeCl2 in n-butanol, stirred at 80°C for 12 h; cooled to room temp., concd., pptd.(Et2O), washed (Et2O), dried (vac.), elem. anal.;

DOI:10.1016/j.molcata.2006.10.028

upstream raw materials:

2,6-[(2,6-iPr₂C₆H₃)NC(CH(CH₃)2)]2C₅H₃N

water