phosphorane, triphenyl-, oxide, cobalt(2+) salt, compd. with trihydroxyoxochlorine (4:1:1)

Base Information

• Chemical Name: phosphorane, triphenyl-, oxide, cobalt(2+) salt, compd. with trihydroxyoxochlorine (4:1:1)
• CAS No.: 52242-87-2
• Molecular Formula: C₇₂H₆₀CoO₄P₄*2ClO₄
• Molecular Weight: 1371.06

Synonyms:

Chemical Property of phosphorane, triphenyl-, oxide, cobalt(2+) salt, compd. with trihydroxyoxochlorine (4:1:1)

Chemical Property:

• Vapor Pressure: 2.62E-08mmHg at 25°C

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phosphorane, triphenyl-, oxide, cobalt(2+) salt, compd. with trihydroxyoxochlorine (4:1:1)

There total 3 articles about phosphorane, triphenyl-, oxide, cobalt(2+) salt, compd. with trihydroxyoxochlorine (4:1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.2%

cobalt(II) perchlorate * 5 H2O + Triphenylphosphine oxide (791-28-6) → Co(II)(triphenylphosphine oxide)4(ClO4)2 (52242-87-2)

Guidance literature:

In acetone; formation by addn. of Co(ClO4)2*5H2O to a soln. of triphenylphosphine oxide in acetone; refluxing for some min; addn. of ether to the hot soln.;; washing with ether/acetone mixt.; drying in vac.;;

Reference yield: 54.0%

tris(cyclohexylisocyanide)bis(triphenylphosphine)cobalt(II) perchlorate → Co(II)(triphenylphosphine oxide)4(ClO4)2 (52242-87-2)

Guidance literature:

In dichloromethane; Irradiation (UV/VIS); dissolving, filtration, 365 nm, 50 h; filtration, pptn. on ether addn., cooling (1 h), filtration, washing (ether), partial evapn. (overnight), dissolving in CH2Cl2, filtration, pptn. on dropwise ether addn., cooling in ice (45 min), filtration, washing (ether); elem. anal.;

DOI:10.1080/00945719708003157

Reference yield:

cobalt(II) perchlorate hexahydrate + Triphenylphosphine oxide (791-28-6) → Co(II)(triphenylphosphine oxide)4(ClO4)2 (52242-87-2)

Guidance literature:

In ethanol; formation by evapn. of a mixt. of MetOH solns. of Co(ClO4)2*6H2O and triphenylphosphine oxide;;

DOI:10.1039/CT9068900262

upstream raw materials:

Triphenylphosphine oxide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 52242-87-2 phosphorane, triphenyl-, oxide, cobalt(2+) salt, compd. with trihydroxyoxochlorine (4:1:1)

Send

Send

Metric Ton KG G Pound L ML

Send

Send