Tris(triethylene glycol monobenzyl ether) phosphate

Base Information

• Chemical Name: Tris(triethylene glycol monobenzyl ether) phosphate
• CAS No.: 158983-51-8
• Molecular Formula: C₃₉H₅₇O₁₃P
• Molecular Weight: 764.848
• Mol file: 158983-51-8.mol

Synonyms:

Chemical Property of Tris(triethylene glycol monobenzyl ether) phosphate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Tris(triethylene glycol monobenzyl ether) phosphate

There total 3 articles about Tris(triethylene glycol monobenzyl ether) phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl chloride (100-44-7) → Tris(triethylene glycol monobenzyl ether) phosphate (158983-51-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 50.4 percent / NaH / tetrahydrofuran / 16 h / Heating

2: NaH, POCl₃ / tetrahydrofuran / 1.) 8 deg C, 30 min

With sodium hydride; trichlorophosphate; In tetrahydrofuran;

DOI:10.1021/jo00104a026

Reference yield:

2,2'-[1,2-ethanediylbis(oxy)]bisethanol (112-27-6) → Tris(triethylene glycol monobenzyl ether) phosphate (158983-51-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 50.4 percent / NaH / tetrahydrofuran / 16 h / Heating

2: NaH, POCl₃ / tetrahydrofuran / 1.) 8 deg C, 30 min

With sodium hydride; trichlorophosphate; In tetrahydrofuran;

DOI:10.1021/jo00104a026

Reference yield:

triethylene glycol monobenzyl ether (55489-58-2,1201808-31-2) → Phosphoric acid mono-{2-[2-(2-benzyloxy-ethoxy)-ethoxy]-ethyl} ester + Phosphoric acid bis-{2-[2-(2-benzyloxy-ethoxy)-ethoxy]-ethyl} ester + Tris(triethylene glycol monobenzyl ether) phosphate (158983-51-8)

Guidance literature:

With sodium hydride; trichlorophosphate; In tetrahydrofuran; Yield given. Yields of byproduct given. Title compound not separated from byproducts; 1.) 8 deg C, 30 min;

DOI:10.1021/jo00104a026

upstream raw materials:

triethylene glycol monobenzyl ether

benzyl chloride

2,2'-[1,2-ethanediylbis(oxy)]bisethanol