Dimethyl <(phenylthio)methyl>malonate

Base Information

Chemical Name:Dimethyl <(phenylthio)methyl>malonate
CAS No.:153180-12-2
Molecular Formula:C₂₁H₂₃NO₅S
Molecular Weight:401.483
Hs Code.:

Dimethyl <N-(3-phenylpropionyl)amino><(phenylthio)methyl>malonate

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Suppliers and Price of Dimethyl <(phenylthio)methyl>malonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dimethyl <(phenylthio)methyl>malonate

Chemical Property:

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Technology Process of Dimethyl <(phenylthio)methyl>malonate

There total 3 articles about Dimethyl <(phenylthio)methyl>malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 153180-27-9
Diethyl malonate

: 153180-12-2
Dimethyl <(phenylthio)methyl>malonate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 2 h

2: NaOMe / TBAB / methanol; dimethylformamide / Ambient temperature

With sodium methylate; tetrabutylammomium bromide; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00073a040

Reference yield:

: 645-45-4
hydrocinnamic acid chloride

: 153180-12-2
Dimethyl <(phenylthio)methyl>malonate

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / K₂CO₃ / CH₂Cl₂; H₂O / 0 deg C to r.t.

2: methanol / 2 h

3: NaOMe / TBAB / methanol; dimethylformamide / Ambient temperature

With sodium methylate; potassium carbonate; tetrabutylammomium bromide; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo00073a040

Reference yield:

: 7205-91-6
phenylthiomethyl chloride

: 2-(3-Phenyl-propionylamino)-malonic acid dimethyl ester

: 153180-12-2
Dimethyl <(phenylthio)methyl>malonate

Guidance literature:: With sodium methylate; tetrabutylammomium bromide; In methanol; N,N-dimethyl-formamide; Yield given; Ambient temperature;
DOI:10.1021/jo00073a040