O(μ-C6H5BNCH3)2CO

Base Information

Chemical Name:O(μ-C6H5BNCH3)2CO
CAS No.:81233-30-9
Molecular Formula:C₁₅H₁₆B₂N₂O₂
Molecular Weight:277.926
Hs Code.:

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Chemical Property of O(μ-C6H5BNCH3)2CO

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Technology Process of O(μ-C6H5BNCH3)2CO

There total 3 articles about O(μ-C6H5BNCH3)2CO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 96-31-1
N,N'-Dimethylurea

: 873-51-8
phenylborondichloride

: 84185-28-4
2-n-Butyl-2,3,5,6-tetrahydro-3,5-dimethyl-6-phenyl-4H-1,3,5,2,6-oxadiazadiborin-4-on

: 81233-30-9
O(μ-C6H5BNCH3)2CO

Guidance literature:: With n-butyllithium; In hexane; Petroleum ether; byproducts: butane, LiBr; the urea in petroleum ether was refluxed under N2 with n-BuLi in hexanefor 48 h; the solvents were removed in vac., the residue was fractional distd.; elem. anal.;

Reference yield: 70.0%

: 96-31-1
N,N'-Dimethylurea

: 873-51-8
phenylborondichloride

: 81233-30-9
O(μ-C6H5BNCH3)2CO

: (Cl)B(CH₃)NCO(CH₃)NCO(CH₃)N

: (Cl)B(CH₃)N(Cl)B(CH₃)NCO(CH₃)N

: (C₆H₅)B(CH₃)N(Cl)B(CH₃)NCO(CH₃)N

: 81233-29-6
3,5-Dimethyl-2,6-diphenyl-1,3,5-triaza-2,6-dibora-cyclohexanon-4

Guidance literature:: In tetrachloromethane; byproducts: HCl; edducts refluxed under N2 in 1:1 ratio for 24 h; evapd. in vac., sublimation in vac., elem. anal., other products detected by MAS.;
DOI:10.1016/S0022-328X(00)89013-0

Reference yield:

: 124357-26-2
O(μ-C6H5BNCH3)2CO*(CH3)2NH

: 81233-30-9
O(μ-C6H5BNCH3)2CO

Guidance literature:: In neat (no solvent); byproducts: (CH3)2NH; under inert atm., heating of B-compound above melting point until evolution of (CH3)2NH; distd. under vac., sublimation, slowly crystn. on standing;