Mo(C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅))(CO)3

Base Information

Chemical Name:Mo(C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅))(CO)3
CAS No.:127065-59-2
Molecular Formula:C₃₀H₃₃MoN₃O₃
Molecular Weight:579.55
Hs Code.:

Mo(C<sub>2</sub>H<sub>4</sub>N(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)C<sub>2</sub>H<sub>4</sub>N(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)C<sub>2</sub>H<sub>4</sub>N(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>))(CO)3

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Chemical Property of Mo(C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅))(CO)3

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Technology Process of Mo(C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅))(CO)3

There total 2 articles about Mo(C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅))(CO)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 125262-43-3
N,N',N''-tribenzyl-1,4,7-triazacyclononane

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 127065-59-2
Mo(C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅))(CO)3

Guidance literature:: In acetonitrile; byproducts: CO; refluxing a mixture of Mo(CO)6 and the ligand in acetonitrile for 5 h under Ar, cooling to 5°C; filtn. of ppt., washing (ether), drying, elem. anal.;

Reference yield:

: 127065-64-9
Mo(C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅))(CO)3⁽¹⁺⁾*PF₆^(1-)={Mo(C₂H₄N(CH₂C₆H₅))3(CO)3}(PF₆)

: 127065-59-2
Mo(C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅))(CO)3

Guidance literature:: With P(C₆H₅)3; In dichloromethane; addn. of PPh3 to a soln. of the starting complex in CH2Cl2, refluxing under Ar for 1 h; monitored by IR;

Reference yield: 80.0%

: ferrocenium hexafluorophosphate

: 127065-59-2
Mo(C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅))(CO)3

: 1643-19-2
tetrabutylammomium bromide

: 127065-72-9
Mo(C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅)C₂H₄N(CH₂C₆H₅))(CO)3(Br)⁽¹⁺⁾*PF₆^(1-)={Mo(C₂H₄N(CH₂C₆H₅))3(CO)3(Br)}(PF₆)

Guidance literature:: In dichloromethane; addn. of the ferrocenium-salt to a soln. of the starting complex in CH2Cl2, addn. of (TBA)Br, stirring for 10 min; monitored by IR, pptg. by addn. of diethyl ether;