carbonylosmium(II) 5,10,15,20-tetraphenylporphyrinate monomethanol complex

Base Information

Chemical Name:carbonylosmium(II) 5,10,15,20-tetraphenylporphyrinate monomethanol complex
CAS No.:117853-39-1
Molecular Formula:C₄₆H₃₂N₄O₂Os
Molecular Weight:862.986
Hs Code.:

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Chemical Property of carbonylosmium(II) 5,10,15,20-tetraphenylporphyrinate monomethanol complex

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Technology Process of carbonylosmium(II) 5,10,15,20-tetraphenylporphyrinate monomethanol complex

There total 1 articles about carbonylosmium(II) 5,10,15,20-tetraphenylporphyrinate monomethanol complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104677-48-7
carbonylosmium(II) 5,10,15,20-tetraphenylporphyrinate

: 117853-39-1
carbonylosmium(II) 5,10,15,20-tetraphenylporphyrinate monomethanol complex

Guidance literature:: With methanol; In methanol; dichloromethane; recrystn. from CH2Cl2-CH3OH; elem. anal.;;

Reference yield: 83.0%

: 117853-39-1
carbonylosmium(II) 5,10,15,20-tetraphenylporphyrinate monomethanol complex

: 222165-16-4
N,N-dimethyl-4-((1E,3E)-4-(pyridin-4-yl)buta-1,3-dienyl)aniline

: carbonyl (5,10,15,20-tetraphenylphorphyrinate)[(1E,3E)-(4-dimethylamino)buta-1,3-dienylstirylpyridine] osmium(II)

Guidance literature:: In chloroform; Os complex dissolved in CHCl3; ligand (1.1 equiv.) added soln.; stirred for 15 min; solvent removed in vac.; washed with H2O; filtered; purified by column chromy. (silica gel, CHCl3); elem. anal.;
DOI:10.1016/j.ica.2005.12.056

Reference yield: 80.0%

: E-4-[2-(4-trifluoromethyl-phenyl)-ethenyl]-pyridine

: 117853-39-1
carbonylosmium(II) 5,10,15,20-tetraphenylporphyrinate monomethanol complex

: carbonyl (5,10,15,20-tetraphenylphorphyrinate)[(1E)-4-(4'-trifluoromethane)stirylpyridine] osmium(II)

Guidance literature:: In chloroform; Os complex dissolved in CHCl3; ligand (1.1 equiv.) added soln.; stirred for 15 min; solvent removed in vac.; washed with H2O; filtered; purified by column chromy. (silica gel, CHCl3); elem. anal.;
DOI:10.1016/j.ica.2005.12.056