10-(4,5-Dimethoxy-2-methyl-3,6-dioxo-cyclohexa-1,4-dienyl)-decanoic acid phenethyl ester

Base Information

Chemical Name:10-(4,5-Dimethoxy-2-methyl-3,6-dioxo-cyclohexa-1,4-dienyl)-decanoic acid phenethyl ester
CAS No.:84978-07-4
Molecular Formula:C₂₇H₃₆O₆
Molecular Weight:456.579
Hs Code.:

Synonyms:

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Chemical Property of 10-(4,5-Dimethoxy-2-methyl-3,6-dioxo-cyclohexa-1,4-dienyl)-decanoic acid phenethyl ester

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Technology Process of 10-(4,5-Dimethoxy-2-methyl-3,6-dioxo-cyclohexa-1,4-dienyl)-decanoic acid phenethyl ester

There total 5 articles about 10-(4,5-Dimethoxy-2-methyl-3,6-dioxo-cyclohexa-1,4-dienyl)-decanoic acid phenethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 58185-99-2
10-(2,3-Dimethoxy-5-methyl-1,4-benzoquinon-6-yl)decanoic acid

: 103-63-9
1-phenyl-2-bromoethane

: 84978-07-4
10-(4,5-Dimethoxy-2-methyl-3,6-dioxo-cyclohexa-1,4-dienyl)-decanoic acid phenethyl ester

Guidance literature:: With silver(l) oxide; In benzene; for 1h; Heating;
DOI:10.1248/cpb.30.2797

Reference yield:

: 6946-46-9
9-ethoxycarbonylnonanoic acid chloride

: 84978-07-4
10-(4,5-Dimethoxy-2-methyl-3,6-dioxo-cyclohexa-1,4-dienyl)-decanoic acid phenethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) AlCl₃, 2.) 25percent methanolic KOH / 1.) nitrobenzene, 0 deg C, 16 h, RT, 1.5 h

2: 55.4 percent / Zn-Hg, conc. HCl / toluene / 15 h / Heating; other reagent: H₂, 5percent Pd/C

3: 97 percent / ON(SO₃K)2, 1percent NaOH / H₂O / 1 h / Ambient temperature

4: 45 percent / Ag₂O / benzene / 1 h / Heating

With hydrogenchloride; potassium hydroxide; sodium hydroxide; aluminium trichloride; potassium nitrososulfonate; mercury; silver(l) oxide; zinc; In water; toluene; benzene;
DOI:10.1248/cpb.30.2797

Reference yield:

: 6443-69-2
3,4,5-trimethoxytoluene

: 84978-07-4
10-(4,5-Dimethoxy-2-methyl-3,6-dioxo-cyclohexa-1,4-dienyl)-decanoic acid phenethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) AlCl₃, 2.) 25percent methanolic KOH / 1.) nitrobenzene, 0 deg C, 16 h, RT, 1.5 h

2: 55.4 percent / Zn-Hg, conc. HCl / toluene / 15 h / Heating; other reagent: H₂, 5percent Pd/C

3: 97 percent / ON(SO₃K)2, 1percent NaOH / H₂O / 1 h / Ambient temperature

4: 45 percent / Ag₂O / benzene / 1 h / Heating

With hydrogenchloride; potassium hydroxide; sodium hydroxide; aluminium trichloride; potassium nitrososulfonate; mercury; silver(l) oxide; zinc; In water; toluene; benzene;
DOI:10.1248/cpb.30.2797