cis-5-Hydroperoxy-2-methoxy-2-methyltetrahydrofuran

Base Information

• Chemical Name: cis-5-Hydroperoxy-2-methoxy-2-methyltetrahydrofuran
• CAS No.: 116972-50-0
• Molecular Formula: C₆H₁₂O₄
• Molecular Weight: 148.159

Synonyms:

Chemical Property of cis-5-Hydroperoxy-2-methoxy-2-methyltetrahydrofuran

Chemical Property:

Purity/Quality:

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Technology Process of cis-5-Hydroperoxy-2-methoxy-2-methyltetrahydrofuran

There total 3 articles about cis-5-Hydroperoxy-2-methoxy-2-methyltetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.5%

5-Hexen-2-one (109-49-9) → 5-Hydroperoxy-5-methoxy-2-pentanon (116972-42-0) + cis-5-Hydroperoxy-2-methoxy-2-methyltetrahydrofuran (116972-50-0) + trans-6-Methoxy-3-methyl-1,2-dioxan-3-ol (116972-44-2) + cis-6-Methoxy-3-methyl-1,2-dioxan-3-ol (116972-43-1)

Guidance literature:

With ozone; In methanol; at -73 ℃; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;

Reference yield: 4.0%

5-Hexen-2-one (109-49-9) → 1-Methyl-2,3,7-trioxabicyclo<2.2.1>heptan (71121-91-0) + 4-oxopentanal (626-96-0) + 4-(1,2,4-Trioxolan-3-yl)-2-butanon (116972-51-1) + cis-5-Hydroperoxy-2-methoxy-2-methyltetrahydrofuran (116972-50-0) + trans-6-Methoxy-3-methyl-1,2-dioxan-3-ol (116972-44-2) + cis-6-Methoxy-3-methyl-1,2-dioxan-3-ol (116972-43-1)

Guidance literature:

With ozone; In methanol; at -73 ℃; Product distribution; other solvent, also with natural rubber;

Reference yield: 4.0%

5-Hexen-2-one (109-49-9) → 1-Methyl-2,3,7-trioxabicyclo<2.2.1>heptan (71121-91-0) + 4-oxopentanal (626-96-0) + trans-5-Hydroperoxy-2-methoxy-2-methyl-tetrahydrofuran (116972-49-7) + cis-5-Hydroperoxy-2-methoxy-2-methyltetrahydrofuran (116972-50-0)

Guidance literature:

With ozone; In methanol; at -73 ℃; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;

upstream raw materials:

5-Hexen-2-one

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