N-(1-Ethyl-1-propenyl)-N-lithiobenzolamin

Base Information

Chemical Name:N-(1-Ethyl-1-propenyl)-N-lithiobenzolamin
CAS No.:74404-03-8
Molecular Formula:C₁₁H₁₄N*Li
Molecular Weight:167.18
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(1-Ethyl-1-propenyl)-N-lithiobenzolamin

Chemical Property:

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Technology Process of N-(1-Ethyl-1-propenyl)-N-lithiobenzolamin

There total 2 articles about N-(1-Ethyl-1-propenyl)-N-lithiobenzolamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 38425-96-6
N-(diethylmethylidene)phenylamine

: 74404-03-8,74404-08-3,75251-07-9
(Z)-N-(1-Ethyl-1-propenyl)-N-lithiobenzolamin

: 74404-03-8,74404-08-3,75251-07-9
(E)-N-(1-Ethyl-1-propenyl)-N-lithiobenzolamin

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -70 ℃; Product distribution; reaction stereospecificity under kinetically or thermodynamically controlled conditions;
DOI:10.1021/ja00529a058

Reference yield:

: 38425-96-6
N-(diethylmethylidene)phenylamine

: 74404-03-8,74404-08-3,75251-07-9
(Z)-N-(1-Ethyl-1-propenyl)-N-lithiobenzolamin

: 74404-03-8,74404-08-3,75251-07-9
(E)-N-(1-Ethyl-1-propenyl)-N-lithiobenzolamin

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -70 ℃; Product distribution; reaction stereospecificity under kinetically or thermodynamically controlled conditions;
DOI:10.1021/ja00529a058

Reference yield:

: 109-72-8,29786-93-4
n-butyllithium

: 74404-03-8,74404-08-3,75251-07-9
N-(1-Ethyl-1-propenyl)-N-lithiobenzolamin

: 7646-85-7,24359-56-6
zinc(II) chloride

: (C₆H₅NCC₂H₅C₂H₄)Zn(C₄H₉)

Guidance literature:: In diethyl ether; ZnCl2 in diethyl ether was added to a soln. of lithium enamide in diethyl ether at 0°C, after 30 min C4H9Li in hexane was added at -78°C (or added dropwise at 0°C), the mixt. was warmed to room temp.; not sepd.;
DOI:10.1021/ja0465193