C₃₉H₂₉N₅O₇S

Base Information

Chemical Name:C₃₉H₂₉N₅O₇S
CAS No.:100899-77-2
Molecular Formula:C₃₉H₂₉N₅O₇S
Molecular Weight:711.755
Hs Code.:

C<sub>39</sub>H<sub>29</sub>N<sub>5</sub>O<sub>7</sub>S

Synonyms:

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Chemical Property of C₃₉H₂₉N₅O₇S

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Technology Process of C₃₉H₂₉N₅O₇S

There total 4 articles about C₃₉H₂₉N₅O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58463-04-0
N6,N6,2'-O,3'-O-tetrabenzoyladenosine

: 100899-77-2
C₃₉H₂₉N₅O₇S

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) methylphosphonic acid, dicyclohexylcarbodiimide, 2.) oxalic acid dihydrate / 1.) dimethyl sulfoxide, RT, 3 h, 2.) methanol, 30 min

2: trimethylsilyl triflate, zinc iodide / tetrahydrofuran / 2 h / Ambient temperature

3: 1.) Br₂, 2.) 1,8-diazabicyclo<5.4.0>undec-7-ene (DBU) / 1.) CH₂Cl₂, -78 deg C, 35 min

With methylphosphonic acid; trimethylsilyl trifluoromethanesulfonate; bromine; oxalic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; zinc(II) iodide; In tetrahydrofuran;
DOI:10.1021/jo00358a017

Reference yield:

: 100899-71-6
N⁶,N⁶,O^2',O^3'-tetrabenzoyladenosine 5'-aldehyde

: 100899-77-2
C₃₉H₂₉N₅O₇S

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilyl triflate, zinc iodide / tetrahydrofuran / 2 h / Ambient temperature

2: 1.) Br₂, 2.) 1,8-diazabicyclo<5.4.0>undec-7-ene (DBU) / 1.) CH₂Cl₂, -78 deg C, 35 min

With trimethylsilyl trifluoromethanesulfonate; bromine; 1,8-diazabicyclo[5.4.0]undec-7-ene; zinc(II) iodide; In tetrahydrofuran;
DOI:10.1021/jo00358a017

Reference yield:

: 100899-70-5
N⁶,N⁶,O^2',O^3'-tetrabenzoyl-5'-deoxy-5'-(N¹,N³-diphenylethylenediamino)adenosine

: 100899-77-2
C₃₉H₂₉N₅O₇S

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / p-toluenesulfonic acid monohydrate / acetone; CH₂Cl₂ / 0.5 h / 0 °C

2: trimethylsilyl triflate, zinc iodide / tetrahydrofuran / 2 h / Ambient temperature

3: 1.) Br₂, 2.) 1,8-diazabicyclo<5.4.0>undec-7-ene (DBU) / 1.) CH₂Cl₂, -78 deg C, 35 min

With trimethylsilyl trifluoromethanesulfonate; bromine; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; zinc(II) iodide; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/jo00358a017