W(CO)5((1,8-bis(dimethylamino)naphthalen-2-yl)diphenylphosphine)

Base Information

Chemical Name:W(CO)5((1,8-bis(dimethylamino)naphthalen-2-yl)diphenylphosphine)
CAS No.:915799-20-1
Molecular Formula:C₃₁H₂₇N₂O₅PW
Molecular Weight:722.39
Hs Code.:

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Chemical Property of W(CO)5((1,8-bis(dimethylamino)naphthalen-2-yl)diphenylphosphine)

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Technology Process of W(CO)5((1,8-bis(dimethylamino)naphthalen-2-yl)diphenylphosphine)

There total 1 articles about W(CO)5((1,8-bis(dimethylamino)naphthalen-2-yl)diphenylphosphine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 915799-17-6
1,8-bis(dimethylamino)-2-(diphenylphosphanyl)-naphthalene

: 14040-11-0
tungsten hexacarbonyl

: 915799-20-1
W(CO)5((1,8-bis(dimethylamino)naphthalen-2-yl)diphenylphosphine)

Guidance literature:: With ONMe₃*2H₂O; In dichloromethane; under N2; W(CO)6 (0.72 mmol), NMe2-contg. compd. (0.72 mmol) and Me3NO*2H2O were dissolved in CH2Cl2 and stirred at room temp. for 3 h; addnl. Me3NO*2H2O was added; the soln. refluxed overnight; the react. was monitored by IR and TLC; the soln. was decanted and the solvent removed by evapn.; preparative TLC (5:1 hexane-thf + a drop of NEt3); pptn. from CH2Cl2-pentane;
DOI:10.1039/b609561e