1-(6,7,9,10,12,13,20,21,23,24,6,27-dodecahydrodibenzo[b,n][1,4,7,10,13,16,19,22]octaoxacyclotetracosin-ylmethyl)-3-ethyl 1,2-methano[60]fullerene-61,61-dicarboxylate

Base Information

• Chemical Name: 1-(6,7,9,10,12,13,20,21,23,24,6,27-dodecahydrodibenzo[b,n][1,4,7,10,13,16,19,22]octaoxacyclotetracosin-ylmethyl)-3-ethyl 1,2-methano[60]fullerene-61,61-dicarboxylate
• CAS No.: 245091-56-9
• Molecular Formula: C₉₀H₃₈O₁₂
• Molecular Weight: 1311.28

Synonyms:

Chemical Property of 1-(6,7,9,10,12,13,20,21,23,24,6,27-dodecahydrodibenzo[b,n][1,4,7,10,13,16,19,22]octaoxacyclotetracosin-ylmethyl)-3-ethyl 1,2-methano[60]fullerene-61,61-dicarboxylate

Chemical Property:

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Useful:

Technology Process of 1-(6,7,9,10,12,13,20,21,23,24,6,27-dodecahydrodibenzo[b,n][1,4,7,10,13,16,19,22]octaoxacyclotetracosin-ylmethyl)-3-ethyl 1,2-methano[60]fullerene-61,61-dicarboxylate

There total 1 articles about 1-(6,7,9,10,12,13,20,21,23,24,6,27-dodecahydrodibenzo[b,n][1,4,7,10,13,16,19,22]octaoxacyclotetracosin-ylmethyl)-3-ethyl 1,2-methano[60]fullerene-61,61-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C90H38O12*C14H15N*F6P(1-)*H(1+) → dibenzylammonium hexafluorophosphate + 1-(6,7,9,10,12,13,20,21,23,24,6,27-dodecahydrodibenzo[b,n][1,4,7,10,13,16,19,22]octaoxacyclotetracosin-ylmethyl)-3-ethyl 1,2-methano[60]fullerene-61,61-dicarboxylate (245091-56-9)

Guidance literature:

In chloroform-d1; [D₃]acetonitrile; at 24.85 ℃; Equilibrium constant; Thermodynamic data;

DOI:10.1039/a903687c

Reference yield: 16.0%

3,5-dimethylphenyl isocyanate (54132-75-1) + 1-(6,7,9,10,12,13,20,21,23,24,6,27-dodecahydrodibenzo[b,n][1,4,7,10,13,16,19,22]octaoxacyclotetracosin-ylmethyl)-3-ethyl 1,2-methano[60]fullerene-61,61-dicarboxylate (245091-56-9) + N-3,5-di-tert-butylbenzyl-N-3-hydroxypropylammonium hexafluorophosphate → C90H38O12*C27H40N2O2*F6P(1-)*H(1+)

Guidance literature:

With dibutyltin(II) dilaurate; In chloroform; at 20 ℃; for 48h;

DOI:10.1016/j.tet.2005.09.149

Reference yield:

dibenzylammonium hexafluorophosphate + 1-(6,7,9,10,12,13,20,21,23,24,6,27-dodecahydrodibenzo[b,n][1,4,7,10,13,16,19,22]octaoxacyclotetracosin-ylmethyl)-3-ethyl 1,2-methano[60]fullerene-61,61-dicarboxylate (245091-56-9) → C90H38O12*C14H15N*F6P(1-)*H(1+)

Guidance literature:

In chloroform-d1; [D₃]acetonitrile; at 24.85 ℃; Equilibrium constant; Thermodynamic data;

DOI:10.1039/a903687c

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