(η5-C5H4COOCH2CH=CH2)RhI2PPh3

Base Information

• Chemical Name: (η5-C5H4COOCH2CH=CH2)RhI2PPh3
• CAS No.: 682742-66-1
• Molecular Formula: C₂₇H₂₄I₂O₂PRh
• Molecular Weight: 768.175
• Mol file: 682742-66-1.mol

Synonyms:

Chemical Property of (η5-C5H4COOCH2CH=CH2)RhI2PPh3

Chemical Property:

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Technology Process of (η5-C5H4COOCH2CH=CH2)RhI2PPh3

There total 1 articles about (η5-C5H4COOCH2CH=CH2)RhI2PPh3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

[(η5-C5H4COOCH2CH=CH2)RhI2]2 (682742-62-7) + triphenylphosphine (603-35-0) → (η5-C5H4COOCH2CH=CH2)RhI2PPh3 (682742-66-1)

Guidance literature:

In dichloromethane; to soln. ((η5-C5H4COOCH2CH=CH2)RhI2)2 in CH2Cl2 soln. PPh3 in CH2Cl2was added slowly and stirred overnight; react. mixt. was evapd. to dryness, washed with hexane, and recrystd. from THF-hexane; elem. anal.;

DOI:10.1016/j.jorganchem.2003.11.031

upstream raw materials:

[(η5-C5H4COOCH2CH=CH2)RhI2]2

triphenylphosphine