Technology Process of C24H26N2O
There total 8 articles about C24H26N2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
for 3h;
Yield given;
Ambient temperature;
DOI:10.1021/jm00364a027
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) n-butyllithium / 1.) THF, -80 deg C, 1 h, 2.) THF, RT, 1 h
2: 20 percent / sodium hydride / dimethylformamide / 3 h / Heating
3: 80 percent / potassium carbonate / benzene / 20 h / Heating
4: 75 percent / aq. KOH / propan-1-ol / 20 h / Heating
5: triethylamine / CH2Cl2 / 20 h / Ambient temperature
6: lithium aluminum hydride / tetrahydrofuran / 3 h / Ambient temperature
With
potassium hydroxide; lithium aluminium tetrahydride; n-butyllithium; sodium hydride; potassium carbonate; triethylamine;
In
tetrahydrofuran; propan-1-ol; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00364a027
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) n-butyllithium / 1.) THF, -80 deg C, 1 h, 2.) THF, RT, 1 h
2: 20 percent / sodium hydride / dimethylformamide / 3 h / Heating
3: 80 percent / potassium carbonate / benzene / 20 h / Heating
4: 75 percent / aq. KOH / propan-1-ol / 20 h / Heating
5: triethylamine / CH2Cl2 / 20 h / Ambient temperature
6: lithium aluminum hydride / tetrahydrofuran / 3 h / Ambient temperature
With
potassium hydroxide; lithium aluminium tetrahydride; n-butyllithium; sodium hydride; potassium carbonate; triethylamine;
In
tetrahydrofuran; propan-1-ol; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00364a027
