cyclo-[(Me2Si-η5-C5H4)Fe(CO)2(Ph2Si-η5-C5H4)Fe(CO)2]

Base Information

Chemical Name:cyclo-[(Me2Si-η5-C5H4)Fe(CO)2(Ph2Si-η5-C5H4)Fe(CO)2]
CAS No.:959428-23-0
Molecular Formula:C₂₈H₂₄Fe₂O₄Si₂
Molecular Weight:592.361
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyclo-[(Me2Si-η5-C5H4)Fe(CO)2(Ph2Si-η5-C5H4)Fe(CO)2]

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Technology Process of cyclo-[(Me2Si-η5-C5H4)Fe(CO)2(Ph2Si-η5-C5H4)Fe(CO)2]

There total 2 articles about cyclo-[(Me2Si-η5-C5H4)Fe(CO)2(Ph2Si-η5-C5H4)Fe(CO)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 945654-40-0
(η5,η5-C5H4CH2SiMe2C5H4)Fe2(CO)4

: 959428-23-0
cyclo-[(Me2Si-η5-C5H4)Fe(CO)2(Ph2Si-η5-C5H4)Fe(CO)2]

Guidance literature:: In xylene; (N2 or Ar); refluxing a mixt. of iron complex and p-xylene for 8 h with stirring, cooling to room temp.; evapn. in vac., dissolving in CH2Cl2, column chromy. (alumina, petroleumether); elem. anal.;
DOI:10.1021/om8005905

Reference yield: 24.0%

: 13463-40-6,37220-42-1
iron pentacarbonyl

: C₅H₅Si(CH₃)2Si(C₆H₅)2C₅H₅

: 945654-40-0
(η5,η5-C5H4CH2SiMe2C5H4)Fe2(CO)4

: 959428-23-0
cyclo-[(Me2Si-η5-C5H4)Fe(CO)2(Ph2Si-η5-C5H4)Fe(CO)2]

Guidance literature:: In xylene; (N2 or Ar); addn. of ligand to p-xylene and Fe(CO)5, reflux for 8 h, cooling to room temp.; evapn. in vac., dissolving in benzene, column chromy. (silica, petroleumether/CH2Cl2 4:1 then 1;1 vol.); elem. anal.;
DOI:10.1021/om8005905