Technology Process of C64H85N11O17
There total 7 articles about C64H85N11O17 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) dicyclohexylcarbodiimide / DMF-chloroform, 1.) -12 deg C, 10 min, 2.) -10 deg C, 40 min, 0 deg C, 1 h, then room temperature, 1 day
2: 60 percent / hydrazine hydrate / methanol / 24 h / Ambient temperature
3: HCl, NaNO2 / H2O; acetic acid / 0.17 h / -10 - -5 °C
4: 1.) triethylamine / 1.) chloroform, 20 min, 2.) DMF-chloroform, -12 deg C, 1 h, 0 deg C, 3 h, then room temperature, 3 h
With
hydrogenchloride; hydrazine hydrate; triethylamine; dicyclohexyl-carbodiimide; sodium nitrite;
In
methanol; water; acetic acid;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) dicyclohexylcarbodiimide / DMF-chloroform, 1.) -12 deg C, 10 min, 2.) -10 deg C, 40 min, 0 deg C, 1 h, then room temperature, 1 day
2: 60 percent / hydrazine hydrate / methanol / 24 h / Ambient temperature
3: HCl, NaNO2 / H2O; acetic acid / 0.17 h / -10 - -5 °C
4: 1.) triethylamine / 1.) chloroform, 20 min, 2.) DMF-chloroform, -12 deg C, 1 h, 0 deg C, 3 h, then room temperature, 3 h
With
hydrogenchloride; hydrazine hydrate; triethylamine; dicyclohexyl-carbodiimide; sodium nitrite;
In
methanol; water; acetic acid;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 60 percent / hydrazine hydrate / methanol / 24 h / Ambient temperature
2: HCl, NaNO2 / H2O; acetic acid / 0.17 h / -10 - -5 °C
3: 1.) triethylamine / 1.) chloroform, 20 min, 2.) DMF-chloroform, -12 deg C, 1 h, 0 deg C, 3 h, then room temperature, 3 h
With
hydrogenchloride; hydrazine hydrate; triethylamine; sodium nitrite;
In
methanol; water; acetic acid;