4,4'-bis([N-(2,6-diisopropylphenyl)-2-(2,6-diisopropylphenylimino)propanamidato-κ2-N,O-(trimethylphosphine)nickel(II)]methyl)-1,1'-biphenyl

Base Information

Chemical Name:4,4'-bis([N-(2,6-diisopropylphenyl)-2-(2,6-diisopropylphenylimino)propanamidato-κ2-N,O-(trimethylphosphine)nickel(II)]methyl)-1,1'-biphenyl
CAS No.:1244696-74-9
Molecular Formula:C₇₄H₁₀₄N₄Ni₂O₂P₂
Molecular Weight:1260.99
Hs Code.:

4,4'-bis([N-(2,6-diisopropylphenyl)-2-(2,6-diisopropylphenylimino)propanamidato-κ2-N,O-(trimethylphosphine)nickel(II)]methyl)-1,1'-biphenyl

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Chemical Property of 4,4'-bis([N-(2,6-diisopropylphenyl)-2-(2,6-diisopropylphenylimino)propanamidato-κ2-N,O-(trimethylphosphine)nickel(II)]methyl)-1,1'-biphenyl

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Technology Process of 4,4'-bis([N-(2,6-diisopropylphenyl)-2-(2,6-diisopropylphenylimino)propanamidato-κ2-N,O-(trimethylphosphine)nickel(II)]methyl)-1,1'-biphenyl

There total 1 articles about 4,4'-bis([N-(2,6-diisopropylphenyl)-2-(2,6-diisopropylphenylimino)propanamidato-κ2-N,O-(trimethylphosphine)nickel(II)]methyl)-1,1'-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: potassium N-(2,6-diisopropylphenyl)-2-(2,6-diisopropylphenylimino)propanamidate

: 1244696-79-4
4,4'-bis([trans-bis(trimethylphosphine)chloronickel(II)]methyl)-1,1'-biphenyl

: 1244696-74-9
4,4'-bis([N-(2,6-diisopropylphenyl)-2-(2,6-diisopropylphenylimino)propanamidato-κ2-N,O-(trimethylphosphine)nickel(II)]methyl)-1,1'-biphenyl

Guidance literature:: In toluene; under inert atm. to suspn. Ni complex in toluene at -35°C soln. Ksalt ligand in toluene was added, stirred at room temp. for 2 h; soln. was filtered through Celite, solvent was removed, residue was dissolved in toluene, layered with pentane and cooled to -35°C for 24h; elem. anal.;
DOI:10.1021/ja1056938