3-O-<3-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl>-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl chloride

Base Information

Chemical Name:3-O-<3-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl>-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl chloride
CAS No.:134136-31-5
Molecular Formula:C₆₀H₆₀ClNO₁₉
Molecular Weight:1134.58
Hs Code.:

3-O-<3-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl>-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl chloride

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Chemical Property of 3-O-<3-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl>-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl chloride

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Technology Process of 3-O-<3-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl>-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl chloride

There total 2 articles about 3-O-<3-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl>-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118466-47-0
allyl 3-O-<3'-O-(3'',4'',6''-tri-O-acetyl-2''-deoxy-2''-phthalimido-β-D-glucopyranosyl)-2'-O-benzoyl-4'-O-benzyl-α-L-rhamnopyranosyl>-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

: 134136-31-5
3-O-<3-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl>-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: Rh(PPh₃)3Cl / ethanol; H₂O / 12 h / Heating

2: yellow HgO, HgCl₂ / acetone; H₂O / 12 h

3: 98 percent / oxylyl chloride, DMF / CH₂Cl₂ / 2 h

With hypochlorous anhydride; N,N-dimethyl-formamide; mercury dichloride; mercury(II) oxide; Wilkinson's catalyst; In ethanol; dichloromethane; water; acetone;
DOI:10.1016/0008-6215(91)80123-5

Reference yield:

: C₆₃H₆₅NO₂₀

: 134136-31-5
3-O-<3-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl>-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: yellow HgO, HgCl₂ / acetone; H₂O / 12 h

2: 98 percent / oxylyl chloride, DMF / CH₂Cl₂ / 2 h

With hypochlorous anhydride; N,N-dimethyl-formamide; mercury dichloride; mercury(II) oxide; In dichloromethane; water; acetone;
DOI:10.1016/0008-6215(91)80123-5

Reference yield: 43.4%

: 134136-27-9
8-(methoxycarbonyl)octyl 4-O-benzyl-3-O-(3,4,6-tri-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-α-L-rhamnopyranoside

: 134136-31-5
3-O-<3-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl>-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl chloride

: 134136-32-6
C₁₁₈H₁₂₆N₂O₃₂

Guidance literature:: With 4 A molecular sieve; silver trifluoromethanesulfonate; tetramethylurea; In dichloromethane; for 48h; Ambient temperature;
DOI:10.1016/0008-6215(91)80123-5