(S)-6-Benzyloxycarbonylamino-2-((S)-6-benzyloxycarbonylamino-2-{2-[(S)-6-benzyloxycarbonylamino-2-((S)-6-benzyloxycarbonylamino-2-formylamino-hexanoylamino)-hexanoylamino]-acetylamino}-hexanoylamino)-hexanoic acid methyl ester

Base Information

• Chemical Name: (S)-6-Benzyloxycarbonylamino-2-((S)-6-benzyloxycarbonylamino-2-{2-[(S)-6-benzyloxycarbonylamino-2-((S)-6-benzyloxycarbonylamino-2-formylamino-hexanoylamino)-hexanoylamino]-acetylamino}-hexanoylamino)-hexanoic acid methyl ester
• CAS No.: 92514-89-1
• Molecular Formula: C₆₀H₇₉N₉O₁₅
• Molecular Weight: 1166.34

Synonyms:

Chemical Property of (S)-6-Benzyloxycarbonylamino-2-((S)-6-benzyloxycarbonylamino-2-{2-[(S)-6-benzyloxycarbonylamino-2-((S)-6-benzyloxycarbonylamino-2-formylamino-hexanoylamino)-hexanoylamino]-acetylamino}-hexanoylamino)-hexanoic acid methyl ester

Chemical Property:

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Useful:

Technology Process of (S)-6-Benzyloxycarbonylamino-2-((S)-6-benzyloxycarbonylamino-2-{2-[(S)-6-benzyloxycarbonylamino-2-((S)-6-benzyloxycarbonylamino-2-formylamino-hexanoylamino)-hexanoylamino]-acetylamino}-hexanoylamino)-hexanoic acid methyl ester

There total 7 articles about (S)-6-Benzyloxycarbonylamino-2-((S)-6-benzyloxycarbonylamino-2-{2-[(S)-6-benzyloxycarbonylamino-2-((S)-6-benzyloxycarbonylamino-2-formylamino-hexanoylamino)-hexanoylamino]-acetylamino}-hexanoylamino)-hexanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-methyl 2-amino-6-(benzyloxycarbonylamino)hexanoate (24498-31-5) → (S)-6-Benzyloxycarbonylamino-2-((S)-6-benzyloxycarbonylamino-2-{2-[(S)-6-benzyloxycarbonylamino-2-((S)-6-benzyloxycarbonylamino-2-formylamino-hexanoylamino)-hexanoylamino]-acetylamino}-hexanoylamino)-hexanoic acid methyl ester (92514-89-1)

Guidance literature:

Multi-step reaction with 4 steps

1: 1.) dicyclohexylcarbodiimide / DMF-chloroform, 1.) -12 deg C, 10 min, 2.) -10 deg C, 40 min, 0 deg C, 1 h, then room temperature, 1 day

2: 60 percent / hydrazine hydrate / methanol / 24 h / Ambient temperature

3: HCl, NaNO₂ / H₂O; acetic acid / 0.17 h / -10 - -5 °C

4: 1.) triethylamine / chloroform, 1.) 20 min, 2.) -12 deg C, 1 h, 0 deg C, 3 h, then room temperature, 3 h

With hydrogenchloride; hydrazine hydrate; triethylamine; dicyclohexyl-carbodiimide; sodium nitrite; In methanol; water; acetic acid;

Reference yield:

Nα-formyl-NΕ-CBZ-L-lysine (53917-47-8) → (S)-6-Benzyloxycarbonylamino-2-((S)-6-benzyloxycarbonylamino-2-{2-[(S)-6-benzyloxycarbonylamino-2-((S)-6-benzyloxycarbonylamino-2-formylamino-hexanoylamino)-hexanoylamino]-acetylamino}-hexanoylamino)-hexanoic acid methyl ester (92514-89-1)

Guidance literature:

Multi-step reaction with 4 steps

1: 1.) dicyclohexylcarbodiimide / DMF-chloroform, 1.) -12 deg C, 10 min, 2.) -10 deg C, 40 min, 0 deg C, 1 h, then room temperature, 1 day

2: 60 percent / hydrazine hydrate / methanol / 24 h / Ambient temperature

3: HCl, NaNO₂ / H₂O; acetic acid / 0.17 h / -10 - -5 °C

4: 1.) triethylamine / chloroform, 1.) 20 min, 2.) -12 deg C, 1 h, 0 deg C, 3 h, then room temperature, 3 h

With hydrogenchloride; hydrazine hydrate; triethylamine; dicyclohexyl-carbodiimide; sodium nitrite; In methanol; water; acetic acid;

Reference yield:

Nα-formyl-Nε-Z-L-lysyl-Nε-Z-L-lysine (3059-15-2) → (S)-6-Benzyloxycarbonylamino-2-((S)-6-benzyloxycarbonylamino-2-{2-[(S)-6-benzyloxycarbonylamino-2-((S)-6-benzyloxycarbonylamino-2-formylamino-hexanoylamino)-hexanoylamino]-acetylamino}-hexanoylamino)-hexanoic acid methyl ester (92514-89-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 60 percent / hydrazine hydrate / methanol / 24 h / Ambient temperature

2: HCl, NaNO₂ / H₂O; acetic acid / 0.17 h / -10 - -5 °C

3: 1.) triethylamine / chloroform, 1.) 20 min, 2.) -12 deg C, 1 h, 0 deg C, 3 h, then room temperature, 3 h

With hydrogenchloride; hydrazine hydrate; triethylamine; sodium nitrite; In methanol; water; acetic acid;

upstream raw materials:

[(S)-5-Azidocarbonyl-5-((S)-6-benzyloxycarbonylamino-2-formylamino-hexanoylamino)-pentyl]-carbamic acid benzyl ester

(S)-methyl 2-amino-6-(benzyloxycarbonylamino)hexanoate

N^α-formyl-N^Ε-CBZ-L-lysine

N^α-formyl-N^ε-Z-L-lysyl-N^ε-Z-L-lysine

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