3-(Phenyl-pyrrolidin-1-yl-methyl)-pyridazine

Base Information

Chemical Name:3-(Phenyl-pyrrolidin-1-yl-methyl)-pyridazine
CAS No.:127478-23-3
Molecular Formula:C₁₅H₁₇N₃
Molecular Weight:239.32
Hs Code.:

Synonyms:

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Chemical Property of 3-(Phenyl-pyrrolidin-1-yl-methyl)-pyridazine

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Technology Process of 3-(Phenyl-pyrrolidin-1-yl-methyl)-pyridazine

There total 7 articles about 3-(Phenyl-pyrrolidin-1-yl-methyl)-pyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37542-92-0
2-benzylfuran

: 127478-23-3
3-(Phenyl-pyrrolidin-1-yl-methyl)-pyridazine

Guidance literature:: Multi-step reaction with 6 steps

1: 85 percent / sodium bromide / 6 h / -5 °C / electrochemical oxidation, 12 V (0.6 A)

2: 40 percent / hydrazine hydrochloride, sodium pyrophosphate / propan-1-ol / 10 h / Heating; pH=6.5

3: 85 percent / selenium dioxide / acetic acid / 1 h / 100 °C

4: 95 percent / sodium borohydride / methanol / 1 h / Ambient temperature

5: 84 percent / thionyl chloride / toluene / 12 h / Ambient temperature

6: 65 percent / toluene / 6 h / Heating

With sodium pyrophosphate; sodium tetrahydroborate; selenium(IV) oxide; thionyl chloride; hydrazine hydrochloride; sodium bromide; In methanol; propan-1-ol; acetic acid; toluene;

Reference yield:

: 63540-69-2
2-benzyl-2,5-dimethoxy-2,5-dihydro-furan

: 127478-23-3
3-(Phenyl-pyrrolidin-1-yl-methyl)-pyridazine

Guidance literature:: Multi-step reaction with 5 steps

1: 40 percent / hydrazine hydrochloride, sodium pyrophosphate / propan-1-ol / 10 h / Heating; pH=6.5

2: 85 percent / selenium dioxide / acetic acid / 1 h / 100 °C

3: 95 percent / sodium borohydride / methanol / 1 h / Ambient temperature

4: 84 percent / thionyl chloride / toluene / 12 h / Ambient temperature

5: 65 percent / toluene / 6 h / Heating

With sodium pyrophosphate; sodium tetrahydroborate; selenium(IV) oxide; thionyl chloride; hydrazine hydrochloride; In methanol; propan-1-ol; acetic acid; toluene;

Reference yield:

: 60905-93-3
3-benzyl-pyridazine

: 127478-23-3
3-(Phenyl-pyrrolidin-1-yl-methyl)-pyridazine

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / selenium dioxide / acetic acid / 1 h / 100 °C

2: 95 percent / sodium borohydride / methanol / 1 h / Ambient temperature

3: 84 percent / thionyl chloride / toluene / 12 h / Ambient temperature

4: 65 percent / toluene / 6 h / Heating

With sodium tetrahydroborate; selenium(IV) oxide; thionyl chloride; In methanol; acetic acid; toluene;