methyl>diphenylphosphanoxid

Base Information

• Chemical Name: methyl>diphenylphosphanoxid
• CAS No.: 96617-95-7
• Molecular Formula: C₂₇H₂₁N₂O₂P
• Molecular Weight: 436.45
• Mol file: 96617-95-7.mol

Synonyms:

Chemical Property of methyl>diphenylphosphanoxid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl>diphenylphosphanoxid

There total 2 articles about methyl>diphenylphosphanoxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

7-(2-Propinyloxy)benzocycloheptenylium-perchlorat (96617-92-4) + diphenylphosphorylazide (5353-66-2) → benzocyclohepten-7-one (4443-91-8) + methyl>diphenylphosphanoxid (96617-95-7)

Guidance literature:

With triethylamine; In dichloromethane; for 0.25h; Ambient temperature;

Reference yield:

7-(2-Propinyloxy)benzocycloheptenylium-perchlorat (96617-92-4) + diphenylphosphorylazide (5353-66-2) → methyl>diphenylphosphanoxid (96617-95-7)

Guidance literature:

Yield given;

Reference yield: 90.0%

methyl>diphenylphosphanoxid (96617-95-7) → C27H21N2O2P (96617-98-0)

Guidance literature:

In acetonitrile; for 72h; Ambient temperature;

upstream raw materials:

7-(2-Propinyloxy)benzocycloheptenylium-perchlorat

diphenylphosphorylazide

Downstream raw materials:

C₂₇H₂₁N₂O₂P

C₂₇H₂₁N₂O₂P

6c-(Diphenyl-phosphinoyl)-1-propa-1,2-dienyl-2a,2b,6b,6c-tetrahydro-1H-benzo[a]cyclopropa[cd]pentalen-2-one

(1S,6bR,6cR)-6c-(Diphenyl-phosphinoyl)-1-propa-1,2-dienyl-2a,2b,6b,6c-tetrahydro-1H-benzo[a]cyclopropa[cd]pentalen-2-one