(2-Azido-phenyl)-(2,4,6-trimethyl-phenyl)-methanone

Base Information

Chemical Name:(2-Azido-phenyl)-(2,4,6-trimethyl-phenyl)-methanone
CAS No.:87895-68-9
Molecular Formula:C₁₆H₁₅N₃O
Molecular Weight:265.315
Hs Code.:

Synonyms:

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Chemical Property of (2-Azido-phenyl)-(2,4,6-trimethyl-phenyl)-methanone

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Technology Process of (2-Azido-phenyl)-(2,4,6-trimethyl-phenyl)-methanone

There total 4 articles about (2-Azido-phenyl)-(2,4,6-trimethyl-phenyl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 552-16-9,104810-18-6
ortho-nitrobenzoic acid

: 87895-68-9
(2-Azido-phenyl)-(2,4,6-trimethyl-phenyl)-methanone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) trifluoroacetic anhydride, boron trifluoride-ether / 2.) ice-bath, 2 h

2: 7.5 percent / triethylphosphite / various solvent(s) / 72 h / Heating

3: 1.) conc. HCl, sodium nitrite, 2.) sodium azide, sodium acetate / 1.) acetic acid, water, below 5 deg C

With hydrogenchloride; sodium azide; boron trifluoride diethyl etherate; sodium acetate; trifluoroacetic anhydride; sodium nitrite; triethyl phosphite; In various solvent(s);

Reference yield:

: 71319-22-7
2-nitro-2',4',6'-trimethylbenzophenone

: 87895-68-9
(2-Azido-phenyl)-(2,4,6-trimethyl-phenyl)-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 7.5 percent / triethylphosphite / various solvent(s) / 72 h / Heating

2: 1.) conc. HCl, sodium nitrite, 2.) sodium azide, sodium acetate / 1.) acetic acid, water, below 5 deg C

With hydrogenchloride; sodium azide; sodium acetate; sodium nitrite; triethyl phosphite; In various solvent(s);

Reference yield:

: 108-67-8
1,3,5-trimethyl-benzene

: 87895-68-9
(2-Azido-phenyl)-(2,4,6-trimethyl-phenyl)-methanone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) trifluoroacetic anhydride, boron trifluoride-ether / 2.) ice-bath, 2 h

2: 7.5 percent / triethylphosphite / various solvent(s) / 72 h / Heating

3: 1.) conc. HCl, sodium nitrite, 2.) sodium azide, sodium acetate / 1.) acetic acid, water, below 5 deg C

With hydrogenchloride; sodium azide; boron trifluoride diethyl etherate; sodium acetate; trifluoroacetic anhydride; sodium nitrite; triethyl phosphite; In various solvent(s);