(η5-pentabenzylcyclopentadienyl)tricarbonylmanganese

Base Information

• Chemical Name: (η5-pentabenzylcyclopentadienyl)tricarbonylmanganese
• CAS No.: 118631-25-7
• Molecular Formula: C₄₃H₃₅MnO₃
• Molecular Weight: 654.687
• Mol file: 118631-25-7.mol

Synonyms:

Chemical Property of (η5-pentabenzylcyclopentadienyl)tricarbonylmanganese

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (η5-pentabenzylcyclopentadienyl)tricarbonylmanganese

There total 1 articles about (η5-pentabenzylcyclopentadienyl)tricarbonylmanganese which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

dimanganese decacarbonyl (10170-69-1) + 1,2,3,4,5-pentabenzyl-1,3-cyclopentadiene (67209-29-4) → (η5-pentabenzylcyclopentadienyl)tricarbonylmanganese (118631-25-7)

Guidance literature:

In xylene; soln. in three-necked flask equipped with gas inlet tube, magnetic stirrer, reflux condenser stirred at reflux (48 h, Ar); filtered (Ar), solvent of filtrate removed, hot hexane added, hot filtered, filtrate concd. to about one third volume, cooled, mother liq. of crystals concd. to afford additional crystals; elem. anal.;

DOI:10.1021/om00105a038

upstream raw materials:

dimanganese decacarbonyl

1,2,3,4,5-pentabenzyl-1,3-cyclopentadiene