Technology Process of C23H23FN8O3S
There total 4 articles about C23H23FN8O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
caesium carbonate;
In
acetonitrile;
at 130 ℃;
for 1h;
Microwave irradiation;
DOI:10.1016/j.bmcl.2017.03.090
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane; water / 0.5 h / 130 °C / Microwave irradiation
2: lithium hydroxide; water / propan-1-ol; methanol / 1.5 h / 170 °C / Microwave irradiation
3: caesium carbonate / acetonitrile / 1 h / 130 °C / Microwave irradiation
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; water; potassium carbonate; caesium carbonate; lithium hydroxide;
In
methanol; propan-1-ol; 1,2-dimethoxyethane; water; acetonitrile;
1: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.bmcl.2017.03.090
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium hydroxide; water / propan-1-ol; methanol / 1.5 h / 170 °C / Microwave irradiation
2: caesium carbonate / acetonitrile / 1 h / 130 °C / Microwave irradiation
With
water; caesium carbonate; lithium hydroxide;
In
methanol; propan-1-ol; acetonitrile;
DOI:10.1016/j.bmcl.2017.03.090
